Benchtop synthesis and characterization of air-stable titanocene(IV) complexes from phosphorous- and sulfur-based amino acid analogs

Tetrahedron Letters

Volumn 40, Issue 35, 1999, Pages 6333-6337

  Shackelford, Scott A ^a,b   Shellhamer, Dale F ^a   Heasley, Victor L ^a  

^a Pt Loma Nazarene University   (United States)

^b Alanex Corporation   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMINO ACID DERIVATIVE; PHOSPHORUS; SULFUR; TITANOCENE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL PROCEDURES; CHEMICAL STRUCTURE; MASS SPECTROMETRY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; SYNTHESIS; ULTRAVIOLET SPECTROSCOPY;

EID: 0033609936     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01252-6     Document Type: Article

References (11)

1. (a) Klapötke, T. M.; Köpf, H.; Tornieporth-Oetting, I. C.; White, P. S. Angew. Chem., Int. Ed. Engl. 1994, 33, 1518-1519;
2. (b) Klapötke, T. M.; Köpf, H.; Tornieporth-Oetting, I. C.; White, P. S. Organometallics 1994, 13, 3628-3633;
3. (c) Tornieporth-Oetting, I. C.; White, P. S. Organometallics 1995, 14, 1632-1636;
4. (d) Ritter, S. K. Fluorine Chemistry Branches Out From Its Traditional Focus; Chem. & Eng. News, Feb. 27, 1995, pp. 39-44, which discusses the work in Refs. 1a-c.
5. (a) Jaouen, G.; Vessieres, A.; Butler, I. S. Acc. Chem. Res. 1993, 26, 361-369;
6. (b) Dagani, R. Organometallic Chemistry Opens New Vistas in Medicine, Materials Science; Chem. & Eng. News, Apr. 10, 1995, pp. 32-36, which discusses the work in Ref. 2a.
7. Shoji, H.; Kondo, Y.; Yoshino, N. Langmuir 1996, 12, 921-924.
8. Gottlieb, H. E.; Kotlyar, V.; Nudelman, A. J. Org. Chem. 1997, 62, 7512-7515.
9. 2 multiplet. Integrating this multiplet was done by noting the chemical shift of temperature-dependent HOD peak, then running a second sample without the acetone reference, and using the HOD peak as the reference peak.
10. -1.
11. On two separate runs, this showed as a double peak at 198 and 212, or 198 and 214 nm.