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note
-
Cyclization reaction of 2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-5-O-phenoxy(thiocarbonyl)-D-glucose O-benzyl oximes under the same conditions gave a mixture of the corresponding cyclopentane derivatives in 63% yield with the stereoselectivity as follows (10 : 11 : 12 : 13 = 51 : 13 : 20 : 16).
-
-
-
-
32
-
-
84982373258
-
-
Reaction of 16 with alkylating reagents such as Meerwein reagent and methyl trifrate also gave unsatisfactory results. In addition, treatment of 10b with dichloromethylenedimethyliminium chloride led to a intractable mixture
-
For example, Appel. R, Angew. Chem., Int. Ed., 1975, 14, 801. Reaction of 16 with alkylating reagents such as Meerwein reagent and methyl trifrate also gave unsatisfactory results. In addition, treatment of 10b with dichloromethylenedimethyliminium chloride led to a intractable mixture.
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