J-Resolved HMBC, a new NMR technique for measuring heteronuclear long- range coupling constants

Tetrahedron Letters

Volumn 40, Issue 34, 1999, Pages 6271-6275

  Furihata, Kazuo ^a   Seto, Haruo ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

Heteronuclear long range coupling; HMBC; J resolved HMBC; NMR

Indexed keywords

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL BOND; NONHUMAN; NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; STEREOCHEMISTRY;

EID: 0033588238     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01233-2     Document Type: Article

References (23)

1. Sasaki, M.; Matsumori, N.; Maruyama, T.; Nonomura, T.; Murata, M.; Tachibana, K.; Yasumoto, T. Angew. Chem., Int. Ed. Engl. 1996, 35, 1672-1675. Matsumori, N.; Nonomura, T.; Sasaki, M.; Murata, M.; Tachibana, K.; Satake, M.; Yasumoto, T. Tetrahedron Lett. 1996, 37, 1269-1272.
2. Sasaki, M.; Matsumori, N.; Maruyama, T.; Nonomura, T.; Murata, M.; Tachibana, K.; Yasumoto, T. Angew. Chem., Int. Ed. Engl. 1996, 35, 1672-1675. Matsumori, N.; Nonomura, T.; Sasaki, M.; Murata, M.; Tachibana, K.; Satake, M.; Yasumoto, T. Tetrahedron Lett. 1996, 37, 1269-1272.
3. Sakaki, R.; Kamiya, H.; Murata, M.; Shimamoto, K. J. Am. Chem. Soc. 1998, 119, 4112-4116.
4. Montelino, G. T.; Winkler, M.; Rauenbuehler, P.; Wagner, G. J. Magn. Reson. 1989, 82, 198-204. Kurz, M.; Schmieder, P; Kessler, H. Angew. Chem.. Int. Ed. Engl. 1991, 30, 1329-1331.
5. Montelino, G. T.; Winkler, M.; Rauenbuehler, P.; Wagner, G. J. Magn. Reson. 1989, 82, 198-204. Kurz, M.; Schmieder, P; Kessler, H. Angew. Chem., Int. Ed. Engl. 1991, 30, 1329-1331.
6. Bax, A.; Freeman, R. J. Am. Chem. Soc. 1982, 104, 1099-1100. Seto, H.; Furihata, K.; Otake, N.; Takahashi, S.; Ito, Y.; Haneishi, T. Tetrahedron Lett. 1984, 25, 337-340.
7. Bax, A.; Freeman, R. J. Am. Chem. Soc. 1982, 104, 1099-1100. Seto, H.; Furihata, K.; Otake, N.; Takahashi, S.; Ito, Y.; Haneishi, T. Tetrahedron Lett. 1984, 25, 337-340.
8. Zhu, G.; Bax, A. J. Magn. Reson. 1993, A 104, 353-357. Zhu, G.; Renewick, A.; Bax, A. J. Magn. Reson. 1994, A 110, 257-261.
9. Zhu, G.; Bax, A. J. Magn. Reson. 1993, A 104, 353-357. Zhu, G.; Renewick, A.; Bax, A. J. Magn. Reson. 1994, A 110, 257-261.
10. Bax, A.; Summers, M. F. J. Am. Chem. Soc. 1986, 108, 2093-2094. Summers, M. F.; Marzilli, L. G.; Bax, A. J. Am. Chem. Soc. 1986, 108, 4285-4292. Bax, A.; Marion, D. J. Magn. Reson. 1988, 78, 186-191.
11. Bax, A.; Summers, M. F. J. Am. Chem. Soc. 1986, 108, 2093-2094. Summers, M. F.; Marzilli, L. G.; Bax, A. J. Am. Chem. Soc. 1986, 108, 4285-4292. Bax, A.; Marion, D. J. Magn. Reson. 1988, 78, 186-191.
12. Bax, A.; Summers, M. F. J. Am. Chem. Soc. 1986, 108, 2093-2094. Summers, M. F.; Marzilli, L. G.; Bax, A. J. Am. Chem. Soc. 1986, 108, 4285-4292. Bax, A.; Marion, D. J. Magn. Reson. 1988, 78, 186-191.
13. Hosur, R. V.; Kumar, M. R.; Sheth, A. J. Magn. Reson. 1985, 65, 375-381. Krishnamurthy, V. V. J. Magn. Reson. 1996, B 113, 46-52. Krishnamurthy, V. V. J. Magn. Reson. 1996, A 121, 33-41.
14. Hosur, R. V.; Kumar, M. R.; Sheth, A. J. Magn. Reson. 1985, 65, 375-381. Krishnamurthy, V. V. J. Magn. Reson. 1996, B 113, 46-52. Krishnamurthy, V. V. J. Magn. Reson. 1996, A 121, 33-41.
15. Hosur, R. V.; Kumar, M. R.; Sheth, A. J. Magn. Reson. 1985, 65, 375-381. Krishnamurthy, V. V. J. Magn. Reson. 1996, B 113, 46-52. Krishnamurthy, V. V. J. Magn. Reson. 1996, A 121, 33-41.
16. Nakayama, H.; Furihata, K.; Seto, H.; Otake, N. Tetrahedron Lett. 1981, 22, 5217-5220.
17. 3OD).
18. Bax, A.; Freeman, R. J. Magn. Reson. 1981, 44, 542-561. Rance, M.; Wagner, G.; Sorensen, O. W.; Wuthrich, K.; Ernst, R. R. J. Magn. Reson. 1984, 59, 250-261. Furihata, K.; Seto, H. Tetrahedron Lett. 1998, 39, 7337-7340.
19. Bax, A.; Freeman, R. J. Magn. Reson. 1981, 44, 542-561. Rance, M.; Wagner, G.; Sorensen, O. W.; Wuthrich, K.; Ernst, R. R. J. Magn. Reson. 1984, 59, 250-261. Furihata, K.; Seto, H. Tetrahedron Lett. 1998, 39, 7337-7340.
20. Bax, A.; Freeman, R. J. Magn. Reson. 1981, 44, 542-561. Rance, M.; Wagner, G.; Sorensen, O. W.; Wuthrich, K.; Ernst, R. R. J. Magn. Reson. 1984, 59, 250-261. Furihata, K.; Seto, H. Tetrahedron Lett. 1998, 39, 7337-7340.
21. Seto, H.; Furihata, K.; Saeki, K.; Otake, N.; Kusakabe, Y.; Xu, C.; Clardy, J. Tetrahedron Lett. 1987, 28, 3357-3360.
22. 6).
23. Experimental conditions: (a) J-resolved HMBC-1, n=25, m=0. (b) J-resolved HMBC-2, n=25, m=12. (c) J-resolved HMBC-2, n=25, m=26. Other experimental parameters were the same as for Ref. 12.