Preparation of carbosilane dendrimers and their characterization using 1H/213C/229Si triple resonance 3D NMR methods

Journal of the American Chemical Society

Volumn 121, Issue 2, 1999, Pages 273-279

  Chai, Minghui ^a   Pi, Zhengjie ^a   Tessier, Claire ^a   Rinaldi, Peter L ^a  

^a UNIVERSITY OF AKRON   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DENDRIMER; ORGANIC COMPOUND; POLYMER; SILANE DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYMERIZATION; PROTON NUCLEAR MAGNETIC RESONANCE; TECHNIQUE; THREE DIMENSIONAL IMAGING;

EID: 0033585526     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9831812     Document Type: Article

References (35)

1. (a) van der Made, A. W.; van Leeuwen, P. W. N. M.; de Wilde, J. C.; Brands, R. A. C. Adv. Mater. 1993, 5, 466.
2. (b) Dagani, R. Chem. Eng. News 1996, 74, 20.
3. (c) Service, R. F. Science 1995, 267, 458-459.
4. (d) Newkome, G. R.; Morefield, C. N.; Vögtle, F. Dendritic Molecules; VCH: New York, 1996.
5. (a) Mathias, L. J.; Carothers, T. W. In Advances in Dendritic Macromolecules; Newkome, G. R., Ed.; JAI: Greenwich, Connecticut, 1995; Vol. 2, Chapter 4.
6. (b) Cuadrado, I.; Morán, M.; Losada, J.; Casado, C. M.; Pasual, C.; Alonso, B.; Lobete, F. In Advances in Dendritic Macromolecules; Newkome, G. R., Ed.; JAI: Greenwich, Connecticut, 1995; Vol. 3, Ch. 4.
7. (c) Gudat, D. Angew. Chem., Int. Ed. Engl. 1997, 36, 1951.
8. van der Made, A. W.; van Leeuwen, P. W. N. M. J. Chem. Soc., Chem. Commun. 1992, 1400.
9. (a) Zhou, L.-L.; Roovers, J. Macromolecules 1993, 26, 963.
10. (b) Zhou, L.-L.; Toporowski, P. M.; Roovers, J.; Hadjichristidis, N. Rubber Chem. Technol. 1992, 65, 303.
11. (c) Roovers, J.; Toporowski, P. M.; Zhou, L.-L. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1992, 33(1), 182.
12. (a) Seyferth, D.; Son, D. Y. Organometallics 1994, 13, 2682.
13. (b) Seyferth, D.; Kugita, T. Organometallics 1995, 14, 5362.
14. (a) Ihre, H.; Hult A.; Soederlind, E. J. Am. Chem. Soc. 1996, 118, 6388.
15. (b) Kim, C.; Park, E.; Kang, E. Bull. Korean Chem. Soc. 1996, 17-(7), 592-595.
16. (c) Kim, R. M.; Bernick, A. M.; Champman, K. T. Proc. Natl. Acad. Sci. U.S.A. 1996, 93(19), 10012.
17. (a) van Genderen, M. H. P.; Baars, M. W. P. L.; Elissen-Roman, C.; de Brabander van der Berg, E. M. M.; Meijer, E. W. Polym. Mater. Sci. Eng. 1995, 73, 336.
18. (b) Smith, B. M.; Todd, P.; Bowman, C. N. Polym. Mater. Sci. Eng. 1996, 75, 331.
19. (c) Ponomarenko, S. A. Rebrov, E. A.; Bobrovsky, A. Y.; Boiko, N. I.; Muzafarov, A. M.; Shibaev, V. P. Liq. Cryst. 1996, 21(1), 1.
20. (d) Catalano, V. J.; Parodi, N. Inorg. Chem. 1997, 36, 537.
21. Wooley, K.; Klug, C.; Kowalewski, T.; Schaefer, J. Polym. Mater. Sci. Eng. 1995, 73, 230.
22. Wooley, K.; Klug, C.; Iasaki, K.; Schaefer, J. J. Am. Chem. Soc. 1997, 119(1), 53.
23. Cavanaugh, J.; Fairbrother, W.; Palmer, A. G., III; Skelton, N. Protein NMR Spectroscopy; Academic Press: London, 1995.
24. Li, L.; Rinaldi, P. L. Macromolecules 1996, 29, 4808.
25. Saito, T.; Medesker, R. E.; Harwood: H. J.; Rinaldi, P. L. J. Magn. Reson., Ser. A 1996, 120, 125.
26. Chai, M.; Saito, T.; Pi, Z.; Tessier, C.; Rinaldi, P. L. Macromolecules 1997, 30, 1240.
27. (a) Shriver, D. F.; Drezdzon, M. A. The Manipulation of Air-Sensitive Compounds, 2nd ed.; Wiley: New York, 1986.
28. (b) Errington, R. J. Advanced Practical Inorganic and Metalorganic Chemistry; Blackie Academic & Professional: New York, 1997.
29. Karstedt, B. Q. U.S. Patent 3,775,452, 1973.
30. States, D. J.; Haberkorn, R. A.; Ruben, D. J. J. Magn. Reson. 1982, 48, 286.
31. (a) Mathias, L. J.; Carothers, T. W. J. Am. Chem. Soc. 1991, 113, 4043.
32. (b) Boury, B.; Corriu, R. J. P.; Leclercq, D.; Mutin, P. H.; Planeix, J.-M.; Vioux, A. Organometallics 1991, 10, 1457.
33. Three examples: (a) Wu, Z.; Bienmann, K. Int. J. Mass Spectrom. Ion Processes 1997, 165/166, 349. (b) Frey, H.; Lorenz, K.; Mülhaupt, R. U.; Mayer-Posner, F. J. Macromol. Symp. 1996, 102, 19.
34. Three examples: (a) Wu, Z.; Bienmann, K. Int. J. Mass Spectrom. Ion Processes 1997, 165/166, 349. (b) Frey, H.; Lorenz, K.; Mülhaupt, R. U.; Mayer-Posner, F. J. Macromol. Symp. 1996, 102, 19.
35. (c) Krska, S. W.; Seyferth, D. J. Am. Chem. Soc. 1998, 120, 3604.