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10 While the titer of bleach remained always in the range 3.5-4% during all the time of this study, we observed a dramatic decrease in the NaClO concentration of the 13% solution. Then, all the reactions with the more concentrated solution have been carried out at the same time with a 10.2% solution, immediately after titration. In our experience, the use of bleach is much more practical, requiring no titration providing that a 1.5-2-fold excess is used. On the other hand, it is advisable to titrate the 13% NaClO solution before its use: we are indebted to one referee for warning us about the rapid decline of its titer.
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