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4 are expected to be superparamagnetic at room temperature. As found experimentally in J. Zhang, C. Boyd, and W. Luo [Phys. Rev. Lett. 77, 390 (1996)], when a ferrofluid is diluted so that the particle separation is large (as in the TEM samples we studied), Néel relaxation or superparamagnetic behavior is observed.
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0344056892
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note
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We thank J. Suhan for microtomy sectioning and J. H. Scott for helpful discussions. SAM. thanks NSF for financial support (awards DMR-9285308 and DMR-9500313).
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