Measuring the temperature width of a first-order single crystal to single crystal phase transition using solid-state NMR: Application to the polymorphism of 2-(2,4-dinitrobenzyl)-3-methylpyridine

Journal of the American Chemical Society

Volumn 121, Issue 49, 1999, Pages 11291-11299

  Schmidt, A ^a   Kababya, S ^a   Appel, M ^a   Khatib, S ^a   Botoshansky, M ^a   Eichen, Y ^a  

^a TECHNION ISRAEL INSTITUTE OF TECHNOLOGY   (Israel)

Author keywords

[No Author keywords available]

Indexed keywords

PICOLINE DERIVATIVE;

ARTICLE; CALORIMETRY; CHEMICAL REACTION; CRYSTAL; CRYSTALLOGRAPHY; NUCLEAR MAGNETIC RESONANCE; PHASE TRANSITION; TEMPERATURE; THERMODYNAMICS;

EID: 0033572922     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja991204m     Document Type: Article

References (33)

1. (a) Herbstein, F. H. Varieties of Polymorphism. Presented at the 18th European Crystallographic Meeting, Prague, Czech Republic, August 1998.
2. (b) Threlfall, T. Analyst 1995, 120, 2435.
3. (c) Polymorphism and Polytypism in Crystals; Verma, A. R., Krishna, P., Eds.; Wiley: New York, 1966.
4. (d) Pharm. J. 1998, 261, 150.
5. (e) Gavezzotti, A. Acc. Chem. Res. 1994, 27, 309.
6. (f) Dunitz, J. D.; Berenstein, J. Acc. Chem. Res. 1995, 28, 193.
7. (a) Ubbelohde, A. R. J. Chim. Phys. 1966, 62, 33.
8. (b) Ubbelohde, A. R. Q. Rev. 1957, 11, 246.
9. (c) Ubbelohde, A. R. Z. Phys. Chem. 1963, 37, 183.
10. Frenkel, J. J. Chem. Phys. 1939, 7, 538.
11. (a) Konno, M.; Sato. Y. Acta Crystallogr. B 1975, 31, 2007.
12. (b) Boerio-Goates, J.; Westrum, E. F. J. Mol. Cryst. Liq. Cryst. 1980, 60, 249.
13. (c) Ubbelohde, A. R. Modern Thermodynamical Principles; Oxford University Press: Oxford, UK, 1952.
14. (d) Barrie, P. J.; Groombridge, C. J.; Grossel, M. C.; Weston, S. C. Chem. Commun. 1992, 1216.
15. Scherl, M.; Haarer, D.; Fischer, J.; DeCian, A.; Lehn, J.-M.; Eichen, Y. J. Phys. Chem. 1996, 100, 16175.
16. Sixl, H.; Warta, R. Chem. Phys. 1985, 94, 147.
17. Eichen, Y.; Botoshansky, M.; Peskin, U.; Scherl, M.; Haarer, D.; Khatib, S. J. Am. Chem. Soc. 1997, 119, 7167.
18. (b) Peskin, U.; Khatib, S.; Eichen, Y. Manuscript in preparation.
19. Kababya, S.; Appel, M.; Schmidt, A. Manuscript in Preparation.
20. Wilmet, F.; Ribet, M.; Bernier, P.; Girault, Y.; Elegant, L. Solid State Commun. 1990, 76, 621.
21. Van Gorkom, L. C. M.; Hook, J. M.; Logan, M. B.; Hanna, J. V.; Wasylishen, R. E. Magn. Reson. Chem. 1995, 33, 791.
22. Bielecki, A.; Burum, D. P. J. Magn. Reson. A 1995, 116, 215.
23. Ferguson, D. B.; Haw, J. F. Anal. Chem. 1995, 67, 3342.
24. Kababya, S.; Appel, M.; Khatib, S.; Eichen,; Schmidt, A. Manuscript in preparation.
25. (a) Desiraju, G. R. Angew. Chem., Int. Ed. Engl. 1995, 34, 2311.
26. (b) Langley, P. J.; Hulliger, J.; Thaimattam, R.; Desiraju, G. R. New J. Chem. 1998, 22, 1307.
27. (c) Desiraju, G. R. Acc. Chem. Res. 1996, 29, 441.
28. Khatib, S.; Botoshansky, M.; Eichen, Y. Acta Crystallogr. B 1997, 53, 306.
29. 15N NMR investigation support the existence of two nonequivalent molecules in the asymmetric unit.
30. Gullion T.; Schaefer J. J. Magn. Reson. 1989 81, 196.
31. Hing, A. W.; Vega, S.; Schaefer, J. J. Magn. Reson. 1992, 96, 205.
32. Tekely, P.; Brondeau, J.; Elbayed, K.; Retournard, A.; Canet, D. J. Magn. Reson. 1988, 80, 509.
33. Gutowsky H. S.; Pake, G. E. J. Chem. Phys. 1950, 18, 162.