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33747570580
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The EXSY experiments were carried out with a standard NOESY program in phase-sensitive mode with a 5% random variation of the evolution time to avoid COSY cross-peaks and a mixing time of 0.6 s.
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16
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0001366854
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-4, 0.005, 0.01, 0.015, 0.02, 0.03, 0.04, 0.06, 0.08, and 10.0 s) and a 90° nonselective pulse. The data were analyzed as described in M. L. H. Green, A. Sella, L.-L. Wong, Organometallics 1992, 11, 2650.
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33747570892
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Line-shape analysis was carried out using the standard DNMR6 program: DNMR6, Quantum Chemical Program Exchange (QCPE 633), Indiana University, Bloomington, IN, 1995.
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0001445720
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