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0344712105
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0344280135
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note
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B at 5 K). Intermolecular magnetic interactions in this sample appear to be operative, but further experiments are necessary in order to fully analyze the system.
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30
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0000014413
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0344280134
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note
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kα(λ=0.71073 Å), 20 max = 49.9 . Data were collected on an Enraf-Nonius CAD4 diffractometer and the structure was solved by direct methods using SHELXTL-Plus V5.0 on an SGI INDY R4400-SC computer. All non-hydrogen atoms were refined with anisotropic displacement parameters. Hydrogen atoms were placed in calculated positions and refined as riding atoms with fixed isotropic displacement parameters. For 6017 independent reflections with 1 > 2a(1) and 433 parameters. R1 = 0.058 and wR2 = 0.1181.
-
-
-
-
33
-
-
0344712103
-
-
note
-
Kα (λ = 0.71073 Å), 2θ max = 50.10 . Data were collected on Siemens SMART system and the structure was solved by direct methods using SHELXTL-Plus V5.0 on an SGI INDY R4400-SC computer. All non-hydrogen atoms were refined with anisotropic displacement parameters. Hydrogen atoms were placed in calculated positions and refined as riding atoms with fixed isotropic displacement parameters. For 6038 independent reflections with 1 > 2o(1) and 444 parameters. R1 = 0.0735 and wR2 = 0.1391.
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35
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37049068357
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0032491185
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