Controlled Synthesis of Polymer Brushes by "Living" Free Radical Polymerization Techniques

Macromolecules

Volumn 32, Issue 5, 1999, Pages 1424-1431

  Husseman, Marc ^a   Malmström, Eva E ^a   McNamara, Molly ^a   Mate, Mathew ^a   Mecerreyes, David ^a   Benoit, Didier G ^a   Hedrick, James L ^a   Mansky, Paul ^b   Huang, E ^b   Russell, Thomas P ^b   Hawker, Craig J ^a  

^a IBM ALMADEN RESEARCH CENTER   (United States)

^b UNIVERSITY OF MASSACHUSETTS   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMINES; ESTERS; FREE RADICAL POLYMERIZATION; MOLECULAR STRUCTURE; MOLECULAR WEIGHT; MONOMERS; NICKEL COMPOUNDS; SURFACE PROPERTIES; SYNTHESIS (CHEMICAL); VINYL RESINS;

ALKOXYAMINES; LIVING POLYMERIZATION; POLYDISPERSITY;

BLOCK COPOLYMERS;

EID: 0033537561     PISSN: 00249297     EISSN: None     Source Type: Journal    
DOI: 10.1021/ma981290v     Document Type: Article

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39. The solidified reaction mixture was dissolved in dichloromethane, and the wafers were removed and washed by immersion in a beaker of tetrahydrofuran for 10 min followed by immersion in a beaker of dichloromethane for 1 h. The wafers were then placed in a Soxhlet apparatus and continuously extracted with refluxing dichloromethane for 24 h, removed, and dried under high vacumn for 24 h.
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