Synthesis of centered icosahedral Europium cluster formed by bis(L-prolinato)nickel(II) ligands and isolation of an electrochemically reduced product of its cluster

Chemistry Letters

Volumn , Issue 12, 1999, Pages 1265-1266

  Igarashi, Satoshi ^a   Yukawa, Yasuhiko ^a  

^a NIIGATA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0033474211     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1999.1265     Document Type: Article

References (17)

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14. 1 4: Eu, 6.48; Ni, 15.01%.
15. 4: Eu, 6.28; Ni, 14.55%. Measurements for diffraction data were carried out on a Rigaku AFCTR diffractometer. The structures were solved by a heavy atom method and refined by a full-matrix least-square treatment.
16. -3 tetrabuthylammonium perchlorate was used. The test electrode was a glassy carbon disk electrode (3.0 mm diameter) and the reference electrode was Ag/AgCl/ saturated KCl. Ferrocene was used as an internal reference (ferrocenium/ ferrocene couple was 0.47 V vs. Ag/AgCl/ saturated KCl).
17. +/Fc) was performed with a platinum gauze electrode for 6 h.