메뉴 건너뛰기




Volumn 140, Issue 2, 1999, Pages 482-486

High-Temperature Pulsed-Field-Gradient Multidimensional NMR of Polymers

Author keywords

2D NMR; High temperature; Polyethylene; Polymers; Pulsed field gradients

Indexed keywords

ARTICLE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0033210819     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1999.1868     Document Type: Editorial
Times cited : (15)

References (20)
  • 1
    • 0002616982 scopus 로고
    • Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence
    • L. Muller, Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence, J. Am. Chem. Soc. 101, 4481-4484 (1979).
    • (1979) J. Am. Chem. Soc. , vol.101 , pp. 4481-4484
    • Muller, L.1
  • 2
    • 0000762913 scopus 로고
    • 1 H chemical shifts in natural-abundance samples via multiple quantum coherence
    • 1 H chemical shifts in natural-abundance samples via multiple quantum coherence, J. Am. Chem. Soc. 105, 7188-7190 (1983).
    • (1983) J. Am. Chem. Soc. , vol.105 , pp. 7188-7190
    • Bax, A.1    Griffey, R.G.2    Hawkins, B.L.3
  • 3
    • 0345311216 scopus 로고
    • 13 C assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR
    • 13 C assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR, J. Am. Chem. Soc. 108, 2093-2094 (1986).
    • (1986) J. Am. Chem. Soc. , vol.108 , pp. 2093-2094
    • Bax, A.1    Summers, M.F.2
  • 4
    • 0029309545 scopus 로고
    • Characterization of polyisobutylene-polybutadiene diblocks by HMQC and HMBC
    • M. Tokles, P. A. Keifer, and P. L. Rinaldi, Characterization of polyisobutylene-polybutadiene diblocks by HMQC and HMBC, Macromolecules 28, 3944-3952 (1995).
    • (1995) Macromolecules , vol.28 , pp. 3944-3952
    • Tokles, M.1    Keifer, P.A.2    Rinaldi, P.L.3
  • 6
    • 0001028964 scopus 로고
    • Gradient-enhanced spectroscopy
    • R. E. Hurd, Gradient-enhanced spectroscopy, J. Magn. Reson. 87, 422-428 (1990).
    • (1990) J. Magn. Reson. , vol.87 , pp. 422-428
    • Hurd, R.E.1
  • 7
    • 0344620689 scopus 로고
    • Gradient-enhanced proton-detected heteronuclear multiple-quantum coherence spectroscopy
    • R. E. Hurd and B. K. John, Gradient-enhanced proton-detected heteronuclear multiple-quantum coherence spectroscopy, J. Magn. Reson. 91, 648-653 (1991).
    • (1991) J. Magn. Reson. , vol.91 , pp. 648-653
    • Hurd, R.E.1    John, B.K.2
  • 8
    • 0344017017 scopus 로고
    • The utility of pulsed-field-gradient HMBC for organic structure determination
    • P. L. Rinaldi and P. A. Keifer, The utility of pulsed-field-gradient HMBC for organic structure determination, J. Magn. Reson. 108, 259-262 (1994).
    • (1994) J. Magn. Reson. , vol.108 , pp. 259-262
    • Rinaldi, P.L.1    Keifer, P.A.2
  • 9
    • 0006285263 scopus 로고    scopus 로고
    • Evaluation of 3D NMR experiments for the characterization of polymer structure
    • T. Saito and P. L Rinaldi, Evaluation of 3D NMR experiments for the characterization of polymer structure, J. Magn. Reson. 132, 41-53 (1998).
    • (1998) J. Magn. Reson. , vol.132 , pp. 41-53
    • Saito, T.1    Rinaldi, P.L.2
  • 11
  • 13
    • 0022715902 scopus 로고
    • 13 C FT NMR spectra of low-density polyethylene by the simplex method
    • R
    • 13 C FT NMR spectra of low-density polyethylene by the simplex method, Polymer 27, 677-680 (1986).
    • (1986) Polymer , vol.27 , pp. 677-680
    • Hay, J.N.1    Mills, P.J.2
  • 14
    • 84987187761 scopus 로고
    • 13 C NMR microstructure determinations of low-density polyethylene homopolymers and copolymers
    • 13 C NMR microstructure determinations of low-density polyethylene homopolymers and copolymers, Recl. Tray. Chim. Pays-Bas. 110, 543-552 (1991).
    • (1991) Recl. Tray. Chim. Pays-Bas. , vol.110 , pp. 543-552
    • Randall, J.C.1    Ruff, C.J.2    Kelchtermans, M.3
  • 16
    • 84972924919 scopus 로고
    • 13 carbon nuclear magnetic resonance characterizations of ethylene-based polymers
    • 13 carbon nuclear magnetic resonance characterizations of ethylene-based polymers, Rev. Macromol. Chem. Phys. C29(2&3), 201-317 (1989).
    • (1989) Rev. Macromol. Chem. Phys. , vol.C29 , Issue.2-3 , pp. 201-317
    • Randall, J.C.1
  • 17
    • 24044459801 scopus 로고
    • Carbon-13 magnetic resonance. II. Chemical shift data for the alkanes
    • D. M. Grant and E. G. Paul, Carbon-13 magnetic resonance. II. Chemical shift data for the alkanes, J. Am. Chem. Soc. 86, 2984-2990 (1964).
    • (1964) J. Am. Chem. Soc. , vol.86 , pp. 2984-2990
    • Grant, D.M.1    Paul, E.G.2
  • 19
    • 0006284032 scopus 로고
    • Characterization of long-chain branching in polyethylenes using high-field carbon-13 NMR
    • "Polymer Characterization by ESR and NMR" (A. E. Woodward and F. A. Bovey, Eds.), Am. Chem. Soc., Washington, DC
    • J. C. Randall, Characterization of long-chain branching in polyethylenes using high-field carbon-13 NMR, in "Polymer Characterization by ESR and NMR" (A. E. Woodward and F. A. Bovey, Eds.), ACS Symposium Series, Vol. 142, pp. 93-118, Am. Chem. Soc., Washington, DC (1980).
    • (1980) ACS Symposium Series , vol.142 , pp. 93-118
    • Randall, J.C.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.