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2-EtOH gave pure 3 in 25-30% yield as pale-yellow, fine plates.
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45
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0345434098
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note
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2), 44.5 (C), 46.9 (C), 153.9 (C).
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46
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0344140493
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note
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-3 for 1992 reflections [I ≥ 2σ(I)] (210 parameters). For more details of the X-ray single-crystal analyses, see Supporting Information.
-
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47
-
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0345002976
-
-
4 assumed to be the tetrathiolane 1-oxide and now should read the vic-disulfoxide 3
-
4 assumed to be the tetrathiolane 1-oxide and now should read the vic-disulfoxide 3.
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48
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0001138809
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0345434096
-
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1H NMR with dibenzyl as the internal standard. See Supporting Information for 4 and 5
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