Growth, microstructure, and permeation properties of supported zeolite (MFI) films and membranes prepared by secondary growth

Chemical Engineering Science

Volumn 54, Issue 15-16, 1999, Pages 3521-3531

  Xomeritakis, George ^a   Gouzinis, Anastasios ^a   Nair, Sankar ^a   Okubo, Tatsuya ^b   He, Mingyan ^c   Overney, Rene M ^c   Tsapatsis, Michael ^a  

^a University of Massachusetts at Amherst   (United States)

^b UNIVERSITY OF TOKYO   (Japan)

^c University of Washington   (United States)

Author keywords

Gas permeation; Inorganic membrane; Seeded growth; Silicalite 1; Zeolite membrane

Indexed keywords

ALUMINA; CRYSTAL GROWTH; CRYSTAL MICROSTRUCTURE; FILM GROWTH; MEMBRANES; POLYCRYSTALLINE MATERIALS;

GAS PERMEATION; SECONDARY GROWTH; ZEOLITE MEMBRANE;

ZEOLITES;

FILM; GAS PERMEATION; MEMBRANE; MICROSTRUCTURE; ZEOLITE;

EID: 0033167007     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0009-2509(98)00515-6     Document Type: Article

References (25)

1. Bein, T. (1996). Synthesis and applications molecular sieve layers and membranes. Chem. Mater., 8, 1636-1653.
2. Boudreau, L.C., & Tsapatsis, M. (1997). A highly oriented thin film of zeolite A. Chem. Mater., 9, 1705-1709.
3. Boudreau, L.C., Kuck, J.A., & Tsapatsis, M. (1998). Deposition of oriented zeolite A films: In situ and secondary growth. J. Membr. Sci. 152, 41.
4. Brinker, J.C. (1998). Oriented inorganic films. Curr. Opin. Colloid Interface Sci., 3, 166-173.
5. Burggraaf, A.J., Vroon, Z.A.E.P., Keizer, K., & Verweij, H. (1998). Permeation of single gases in thin zeolite MFI membranes. J. Membr. Sci., 144, 77.
6. Burkett, S.L., & Davis, M.E. (1995a). Mechanisms of structure direction in the synthesis of pure-silica zeolites. 1. Synthesis of TPA/Si-ZSM-5. Chem. Mater., 7, 920-928.
7. Burkett, S.L., & Davis, M.E. (1995b). Mechanisms of structure direction in the synthesis of pure-silica zeolites. 2. Hydrophobic hydration and structural specificity. Chem. Mater., 7, 1453-1463.
8. Coronas, J., Falconer, J.L., & Noble, R.D. (1997). Characterization and permeation properties of ZSM-5 tubular membranes. A.I.Ch.E. J., 43, 1797-1812.
9. 8 isomers in ZSM-5 tubular membranes. Ind. Engng Chem. Res., 37, 166.
10. Dokter, W.H., Van Garderen, H.F., Beelen, T.P.M., Van Santen, R.A., & Bras, W. (1995). Homogeneous versus heterogeneous zeolite nucleation. Angew. Chem. Int. Ed. Engl., 34, 73-75.
11. Geus, E.R., Bekkum, H., Bakker, W.J.W., & Moulijn, J.A. (1993). High-temperature stainless steel supported zeolite (MFI) membranes: Preparation, module construction, and permeation experiments. Microporous Mater., 1, 131-147.
12. Gouzinis, A., & Tsapatsis, M. (1998). On the preferred orientation and microstructural manipulation of molecular sieve films prepared by secondary growth. Chem. Mater. 10, 2497.
13. Koegler, J.H., Bekkum, H., & Jansen, J.C. (1997). Growth model of oriented crystals of zeolite Si-ZSM-5. Zeolites, 19, 262-269.
14. Kusakabe, K., Yoneshige, S., Murata, A., & Morooka, S. (1996). Morphology and gas permeance of ZSM-5-type zeolite membrane formed on a porous α-alumina support tube. J. Memb. Sci., 116, 39.
15. Lai, W.F., Deckman, H.W., McHenry, J.A., & Verduijn, J.P. (1996). Zeolite Layers with Controlled Crystal Width and Preferred Orientation Grown on a Growth Enhancing Layer. International Patent Application WO96/01687.
16. Lovallo, M.C., & Tsapatsis, M. (1996). Preferentially oriented submicron silicalite membranes. A.I.Ch.E. J., 42, 3020-3029.
17. Lovallo, M.C., Tsapatsis, M., & Okubo, T. (1996). Preparation of an asymmetric zeolite L film. Chem. Mater., 8, 1579-1583.
18. Lovallo, M.C., Gouzinis, A., & Tsapatsis, M. (1998). Synthesis and characterization of oriented MFI membranes prepared by secondary growth. A.I.Ch.E. J., 44, 1903-1913.
19. Overney, R.M., & Meyer, E. (1993). Tribological investigations using friction force microscopy. Mater. Res. Soc., 18, 26-34.
20. Vroon, Z.A.E.P., Keizer, K., Gilde, M.J., Verweij, H., & Burggraaf, A.J. (1995). Transport properties of alkanes through ceramic thin MFI membranes. J. Memb. Sci., 113, 293-300.
21. Vroon, Z.A.E.P., Keizer, K., Gilde, M.J., Verweij, H., & Burggraaf, A.J. (1996). Transport properties of alkanes through ceramic thin zeolite MFI membranes. J. Memb. Sci., 113, 293.
22. Vroon, Z.A.E.P., Keizer, K., Gilde, M.J., & Verweij, H. (1998). Preparation and characterization of thin zeolite MFI membranes on porous supports. J. Memb. Sci., 144, 65.
23. Xomeritakis, G., & Tsapatsis, M. (1999). Chem. Mater, (in press).
24. 3. J. Chem. Soc. Chem. Commun., 227-228.
25. Yan, Y., Davis, M.E., & Gavalas, G.R. (1997). Preparation of highly selective zeolite ZSM-5 membranes by a post-synthetic coking treatment. J. Memb. Sci., 123, 95.