Synthesis and characterization of oriented MFI membranes prepared by secondary growth

AIChE Journal

Volumn 44, Issue 8, 1998, Pages 1903-1913

  Lovallo, M C ^a   Gouzinis, A ^a   Tsapatsis, M ^a  

^a NONE

Author keywords

[No Author keywords available]

Indexed keywords

ACTIVATION ENERGY; ALUMINA; CARBON DIOXIDE; CRYSTAL MICROSTRUCTURE; CRYSTAL ORIENTATION; HYDROGEN; METHANE; NITROGEN; OXYGEN; POROUS MATERIALS; SYNTHESIS (CHEMICAL); TEXTURES;

SILICALITE; X RAY DIFFRACTION POLE FIGURE TEXTURE ANALYSIS;

PERMSELECTIVE MEMBRANES;

MEMBRANE; PERMEABILITY; SYNTHESIS;

EID: 0032144680     PISSN: 00011541     EISSN: None     Source Type: Journal    
DOI: 10.1002/aic.690440820     Document Type: Article

References (28)

1. Bakker, W. J. W., F. Kapteijn, J. Poppe, and J. A. Moulijn, “ Permeation Characteristics of a Metal‐Supported Silicalite‐1 Zeolite Membrane,” J. Memb. Sci., 117, 57 (1996).
2. Barrer, R. M., “ Porous Crystal Membranes,” J. Chem. Soc. Faraday Trans., 86, 1123 (1990).
3. Boudreau, L. C., and M. Tsapatsis, “ A Highly Oriented Thin Film Of Zeolite A,” Chem. Mat., 9, 1705 (1997a).
4. Boudreau, L. C., J. A. Kuck, and M. Tsapatsis, “Deposition of Oriented Zeolite A Films: In‐situ and Secondary Growth,” J. Memb. Sci., (1997b, in press).
5. Dunne, J. A., R. Mariwala, M. Rao, S. Sircar, R. J. Gorte, and A. L. Myers, “ Calorimetric Heats of Adsorption and Adsorption Isotherms,” Langmuir, 12, 5888 (1996).
6. Funke, H. H., K. R. Frender, K. M. Green, J. L. Wilwerding, B. A. Sweitzer, J. L. Falconer, and R. D. Noble, “ Influence of Adsorbed Molecules on the Permeation Properties of Silicalite Membranes.” J. Memb. Sci., 129, 77 (1997).
7. Geus, E. R., J. E. Marcel, and H. Bekkum, “ Synthesis and Characterization of Zeolite (MFI) Membranes on Porous Ceramic Supports,” J. Chem. Sci. Faraday Trans., 88, 3101 (1992).
8. Gouzinis, A., and M. Tsapatsis, “On the Preferred Orientation anti Microstructural Manipulation of Molecular Sieve Films Prepared by Secondary Growth,” Chem. Mat., in press.
9. Huijser‐Gerits, E. M. C., and G. D. Rieck, “ Defocusing Effects in the Reflection Technique for the Determination of Preferred Orientation,” J. Appl. Crystallog., 7, 286 (1974).
10. Jia, M. D., K. V. Peinemann, and R. D. Behling, “ Ceramic Zeolite Composite Membranes,” J. Memb. Sci., 82, 15 (1993).
11. Jia, M. D., B. Chen, R. D. Noble, and J. L. Falconer, “ CeramicZeolite Composite Membranes and their Application for Separation on Vapor/Gas Mixtures,” J. Memb. Sci., 90, 1 (1994).
12. Kapteijn, F., W. J. W. Bakker, J. Van De Graaf, G. Zheng, J. Poppe, and J. A. Moulijn, “ Permeation and Separation Behavior of a Silicalite‐1 Membrane,” Catal. Today, 25, 213 (1995).
13. Kusakabe, K., T. Kuroda, A. Murata, and S. Morooka, “ Formation of a Y‐type Zeolite Membrane on a Porous Alpha‐Alumina Tube for Gas Separation,” Ind. Eng. Chem. Res., 36, 649 (1997).
14. Lai, W. F., H. W. Deckman, J. A. McHenry, and J. P. Verduijn. “Zeolite Layers with Controlled Crystal Width and Preferred Orientation Grown on a Growth Enhancing Layer,” International Patent Application, WO 96/01687 (1996).
15. Lovallo, M. C., M. Tsapatsis, and T. Okubo, “ Preparation of an Asymmetric Zeolite L Film,” Chem. Mar., 8, 1579 (1996a).
16. Lovallo, M. C., L. Boudreau, and M. Tsapatsis, “ Preparation of Supported Zeolite Films and Layers: Processing of Zeolite Suspensions and In‐situ Growth from Homogeneous Solutions,” Microporous and Macroporous Materials, J. S. Beck, L. E. Iton, L. E. Corbin, R. F. Lobo, M. E. Davis, S. I. Zones, and S. L. Suib, eds., MRS, Pittsburgh, 431, 225 (1996b).
17. Lovallo, M. C., and M. Tsapatsis, “ Microstructural Characterization of an Oriented Silicalite Film,” Advanced Catalytic Materials III, P. Lendor, M. Ledoux, D. Nagaki, and L. Thompson. eds., MRS. Pittsburgh, in press (1998).
18. Lovallo, M. C., and M. Tsapatsis, “ Preferentially Oriented Submicron Silicalite Membranes,” AIChE J., 42, 3020 (1996).
19. Mintova, S., J. Hedlund, B. Schoeman. V. Valtchev, and J. Sterte. “ Continuous Films of Zeolite ZSM‐5 on Modified Gold Surfaces.” Chem. Cornmun., 15 (1997).
20. Noble, R. D., and J. L. Falconer. “ Silicalite‐1 Zeolite Composite Membranes,” Catal. Today, 25, 209 (1995).
21. Tsapatsis, M., T. Okubo, M. C. Lovallo, and M. E. Davis, “ Synthesis and Structure of Ultrafine Zeolite KI. (LTL) Crystaites and Their Use for Thin Film Zeolite Processing,” Mat. Res. Soc. Symp. Proc., 371, 21 (1995a).
22. Tsapatsis, M., M. C. Lovallo, T. Okubo, M. E. Davis, and M. Sadakata, “ Characterization of Zeolite L Nanoclusters,” Chem. Mat., 7, 1734 (1995b).
23. Tsikoyiannis, J. G., and W. O. Haag, “ Synthesis and Characterization of a Pure Zeolitic Membrane,” Zeolites, 12, 126 (1992).
24. Valtchev, V., B. J. Schoeman, J. Hedlund, S. Mintova, and J. Sterte “ Preparation and Characterization of Hollow Fibers of Silicalite”. Zeolites, 17, 408 (1996).
25. Van der Drift, A., “ Evolutionary Selection, a Principle Governing Growth Orientation in Vapor‐Deposited Layers,” Philips Res. Rep., 22, 267 (1967).
26. Vroon, Z. A. E. P., K. Keizer, M. J. Gilde, I. I. Verweij, and A. J. Burggraaf, “ Transport Properties of Alkanes Through Ceramic Thin MFI Membranes,” J Memb. Sci, 113, 293 (1996).
27. Yan, Y., M. Tsapatsis, G. R. Gavalas, and M. E. Davis, “Zeoljle ZSM‐5 Membranes on Porous α‐Al 2 O 3,” J. Chem. Soc. Chem. Commun., 227 (1995).
28. Yee, A. L., H. C. Ong, L. M. Stewart, and R. P. Chang, “ Development of Flat, Smooth (100) Faceted Diamond Thin Films Using Microwave Plasma Chemical Vapor Deposition,” J. Mat. Res., 12, 1796 (1997).