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note
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The crude MA-H-M was obtained quantitatively, whose NMR and IR spectra showed almost the similar patterns with those after purification, where MA-H-M was obtained in 69% yield.
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27
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0344669775
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note
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On high voltage cellulose-thin layer electrophoresis (850 V, 4°C, 4 min) using a buffer of formic acid acetic acid water (25:75:900, volume ratio), the relative mobility (0.44) of the resulting HAA to L-alanine was the same as that of the threo isomer (0.44) but different from that of the erythro isomer (0.59), which were checked with ninhydrin.
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