Assessment of limits of detection and quantitation using calculation of uncertainty in a new method for water determination

Accreditation and Quality Assurance

Volumn 4, Issue 4, 1999, Pages 124-128

  Kuselman, Ilya ^a   Sherman, Felix ^a  

^a National Physical Laboratory of Israel   (Israel)

Author keywords

Analytical method validation; Karl fischer titration; Limit of detection; Limit of quantitation; Uncertainty of measurements; Water determination

Indexed keywords

EID: 0033106565     PISSN: 09491775     EISSN: None     Source Type: Journal    
DOI: 10.1007/s007690050331     Document Type: Article

References (22)

1. Lauwaars M (1998) Accred Qual Assur 3:32-35
2. USP 23 (1995) The United States Pharmacopeia (USP). The National Formulary. United States Pharmacopeial Convention Inc, Md., USA
3. Kuselman I, Shenhar A (1995) Anal Chim Acta 306:301-305
4. ISO/IEC Guide 25 (1990) General requirements for the competence of calibration and testing laboratories, 3d edn. International Organization for Standardization (ISO), Geneva,
5. CITAC Guide 1 (1995) International guide to quality in analytical chemistry: An aid to accreditation, 1st edn. Teddington, UK
6. EURACHEM (1995) Quantifying uncertainty in analytical measurement, 1st edn. EURACHEM, Teddington, UK
7. Ellison SLS, Williams A (1998) Accred Qual Assur 3:6-10
8. Kuselman I, Shenhar A (1997) Accred Qual Assur 2:180-185
9. Wegscheider W (1997) The Proceedings of the 2nd EURACHEM Workshop "Measurement Uncertainty in Chemical Analysis. Current Practice and Future Directions", 29-30 September, Berlin. EURACHEM
10. Dietrich A (1994) American Lab 26 (5): 33-39
11. Mitchell J Jr, Smith DM (1980) Aquametry, Part III (the Karl Fischer reagent). A treatise on methods for the determination of water. Willey-Interscience, N.Y., USA
12. Margolis SA (1995) Anal Chem 67:4239-4246
13. Margolis SA (1997) Anal Chem 69:4864-4871
14. Zeiler HJ, Heindl R, Wegscheider W (1996) Veitsch-Radex Rundschau 2:48-55
15. Wegscheider W, Zeiler HJ, Heindl R, Mosser J (1997) Ann Chim 87:273-283
16. Sherman F, Kuselman I, Shenhar A (1996) Talanta 43:1035-1042
17. Sherman F, Kuselman I, Shenhar A (1998) Reagent for determining water and ene-diols or thiols. USA Patent No. 5,750,404, 12.05.98
18. Kuselman I (1998) Accred Qual Assur 3:131-133
19. Cedergren A (1996) Anal Chem 68:3679-3681
20. American Public Health Association, American Water Works Association, Water Environment Federation (1995) Standard methods for the examination of water and wastewater, 19th edn. American Public Health Association, Washington, USA, pp 1-10, 1-11
21. Kaus R (1998) Accred Qual Assur 3:150-154
22. Vogelgesang J, Hadrich J (1998) Accred Qual Assur 3:242-255