Sources of Systematic Bias in the Measurement of Water by the Coulometric and Volumetric Karl Fischer Methods

Analytical Chemistry

Volumn 69, Issue 23, 1997, Pages 4864-4871

  Margolis, Sam A ^a  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

OIL; WATER;

ARTICLE; CHEMICAL MODEL; CHEMISTRY; ELECTROCHEMISTRY; METHODOLOGY;

ELECTROCHEMISTRY; MODELS, CHEMICAL; OILS; WATER;

EID: 0031297970     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac9704826     Document Type: Article

References (9)

1. Griffin, P.; Bruce, C.; Christie, J. Minutes of the 55th Annual International Conference of Doble Clients. Doble Engineering Co., Watertown, MA, 1988.
2. ASTM D 1533-88 Standard Test Methods for Water in Insulating Liquids (Karl Fischer Reaction Method). Annu. Book ASTM Stand. 1993, 10.03, 189.
3. Margolis, S. Anal. Chem. 1995, 67, 4239-4246.
4. (a) Hydranal Manual Eugen Scholz Reagents for Karl Fischer Titration; Reidelde-Haen; Dordecht, The Netherlands, 1988.
5. (b) Water Measurement by Karl Fischer Titrimetry; GFS Chemicals Inc.; Powell, OH, 1991.
6. Scholz, E. Karl Fischer Titration Determination of Water, Chemical Laboratory Practice; Springer-Verlag: Berlin, 1984.
7. Gedemer, T.; Frey, R. Am. Lab. 1975, 8 (March), 47-53.
8. 6. Report of Investigation for RM 8509 and RM 8510. NIST: Gaithersbug, MD, 1995.
9. Leo, A.; Hansch, C. J. Org. Chem. 1971, 36, 1539-1544.