Unwanted Signal Leakage in Excitation Sculpting with Single Axis Gradients

Journal of Magnetic Resonance

Volumn 137, Issue 1, 1999, Pages 206-214

  Jerschow, Alexej ^a  

^a UNIVERSITY OF LAUSANNE   (Switzerland)

Author keywords

Coherence pathways; Dipolar demagnetizing field; Excitation sculpting; Pulsed field gradients; Solvent suppression

Indexed keywords

DEUTERIUM OXIDE; WATER;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; COMPARATIVE STUDY; MATHEMATICS; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; THEORETICAL MODEL;

DEUTERIUM OXIDE; MAGNETIC RESONANCE SPECTROSCOPY; MATHEMATICS; MODELS, THEORETICAL; MOLECULAR STRUCTURE; WATER;

EID: 0033092946     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1998.1652     Document Type: Article

References (24)

1. T. L. Hwang and A. J. Shaka, Water suppression that works. Excitation sculpting using arbitrary waveforms and pulsed field gradients, J. Magn. Reson. A 112, 275-279 (1995).
2. K. Stott, J. Stonehouse, J. Keeler, T.-L. Hwang, and A. J. Shaka, Excitation sculpting in high-resolution nuclear magnetic resonance spectroscopy: Application to selective NOE experiments, J. Am. Chem. Soc. 117, 4199-4200 (1995).
3. C. Emetarom, T.-L. Hwang, G. Mackin, and A. J. Shaka, Isotope editing of NMR spectra. Excitation sculpting using BIRD pulses, J. Magn. Reson. A 115, 137-140 (1995).
4. K. Stott, J. Keeler, Q. N. Van, and A. J. Shaka, One-dimensional NOE experiments using pulsed field gradients, J. Magn. Reson. 125, 302-324 (1997).
5. 1H detection, Magn. Reson. Chem. 34, 554-558 (1996).
6. T. Parella, P. Adell, F. Sánchez-Ferrando, and A. Virgili, Effective multiple-solvent suppression scheme using the excitation sculpting principle, Magn. Reson. Chem. 36, 245-249 (1998).
7. Q. N. Van and A. J. Shaka, Improved cross peak detection in two-dimensional proton NMR spectra using excitation sculpting, J. Magn. Reson. 132, 154-158 (1998).
8. C. Dalvit, Efficient multiple-solvent suppression for the study of the interactions of organic solvents with biomolecules, J. Biomol. Nucl. Magn. Reson. 11, 437-444 (1998).
9. M. Mescher, A. Tannus, M. O'Neil Johnson, and M. Garwood, Solvent suppression using selective echo dephasing, J. Magn. Reson. A 123, 226-229 (1996).
10. G. Mackin and A. J. Shaka, Phase-sensitive two-dimensional HMQC and HMQC-TOCSY spectra obtained using double pulsed-field-gradient spin echoes, J. Magn. Reson. A 118, 247-255 (1996).
11. A. Jerschow and N. Müller, Efficient simulation of coherence transfer pathway selection by phase cycling and pulsed field gradients in NMR, J. Magn. Reson. 134, 17-29 (1998).
12. M. E. Rose, "Elementary Theory of Angular Momentum," Wiley, New York (1966).
13. 3He, Phys. Rev. B 19, 5666-5688 (1979).
14. S. Lee, W. Richter, S. Vathyam, and W. S. Warren, Quantum treatment of the effects of dipole-dipole interactions in liquid nuclear magnetic resonance, J. Chem. Phys. 105, 874-900 (1996).
15. M. H. Levitt, Demagnetization field effects in two-dimensional solution NMR, Concepts Magn. Reson. 8, 77-103 (1996).
16. R. Bowtell, R. M. Bowley, and P. Glover, Multiple spin echoes in liquids in a high magnetic field, J. Magn. Reson. 88, 643-651 (1990).
17. W. S. Warren and S. Ahn, The boundary between liquidlike and solidlike behavior in magnetic resonance, J. Chem. Phys. 108, 1313-1325 (1998).
18. J. Jeener, A. Vlassenbroek, and P. Broekaert, Unified derivation of the dipolar field and relaxation terms in the Bloch-Redfield equations of liquid NMR, J. Chem. Phys. 103, 1309-1332 (1995).
19. I. Ardelean, R. Kimmich, S. Stapf, and D. E. Demco, Multiple nonlinear stimulated echoes, J. Magn. Reson. 127, 217-224 (1997).
20. I. Ardelean, S. Stapf, D. E. Demco, and R. Kimmich, The nonlinear stimulated echo, J. Magn. Reson. 124, 506-508 (1997).
21. D. L. Mattiello, W. S. Warren, L. Mueller, and B. T. Farmer II, Minimizing the water resonance in biological NMR: Characterization and suppression of intermolecular dipolar interactions by multiple-axis gradients, J. Am. Chem. Soc. 118, 3253-3261 (1996).
22. 1 field distribution with non-ideal gradients in a high-resolution NMR spectrometer, J. Magn. Reson. 137, 108-115 (1999).
23. A. Vlassenbroek, J. Jeener, and P. Broekaert, Radiation damping in high resolution liquid NMR: A simulation study, J. Chem. Phys. 103, 5886-5897 (1995).
24. X.-A. Mao and C.-H. Ye, Understanding radiation damping in a simple way, Concepts Magn. Reson. 9, 173-187 (1997).