Gradient-enhanced one-dimensional heteronuclear NOE experiment with 1H detection

Magnetic Resonance in Chemistry

Volumn 34, Issue 7, 1996, Pages 554-558

  Stott, Katherine ^a   Keeler, James ^a  

^a UNIVERSITY OF CAMBRIDGE   (United Kingdom)

Author keywords

13C; 1H; DPFGSE; Gibberellic acid; Heteronuclear NOE; NMR; Pulsed field gradients; Quaternary carbon

Indexed keywords

BIOCHEMISTRY;

13C; 1H; DPFGSE; GIBBERELLIC ACID; HETERONUCLEAR; HETERONUCLEAR NOE; ONE-DIMENSIONAL; PULSED FIELD GRADIENTS; QUATERNARY CARBON; SPECTRA'S;

CARBON;

EID: 0030535099     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199607)34:7<554::AID-OMR919>3.0.CO;2-E     Document Type: Article

References (18)

1. D. Neuhaus and M. P. Williamson, The Nuclear Overhauser Effect in Structural and Conformational Analysis. Verlag Chemie, New York (1989).
2. J. K. M. Sanders and J. D. Mersh, Prog. Nucl. Magn. Reson. 15, 353 (1982).
3. A. J. Jones, D. M. Grant and K. F. Kuhlmann, J. Am. Chem. Soc. 91, 5013 (1969).
4. K. Tori, J. Nishikawa and Y. Takeuchi, Tetrahedron Lett. 22, 2793 (1981).
5. K. Kakinuma, N. Imamura, N. Ikekawa, K. Tanaka and S. Minami, J. Am. Chem. Soc. 102, 7493 (1980).
6. R. E. Hurd, J. Magn. Reson. 87, 422 (1990).
7. J. Keeler, R. T. Clowes, A. L. Davis and E. D. Laue, Methods Enzymol. 239C, 145 (1994).
8. W. Bauer, Magn. Reson. Chem. 34, 532 (1996).
9. J. Stonehouse, P. Adell, J. Keeler and A. J. Shaka, J. Am. Chem. Soc. 116, 6037 (1994).
10. K. Stott, J. Stonehouse, T. L. Hwang, J. Keeler and A. J. Shaka, J. Am. Chem. Soc. 117, 4199 (1995).
11. T. L. Hwang and A. J. Shaka, J. Magn. Reson., Ser. A, 112, 275 (1995).
12. A. L. Davis, E. D. Laue, J. Keeler, D. Moskau and J. Lohman, J. Magn. Reson. 94, 637 (1991).
13. R. K. Harris, Nuclear Magnetic Resonance Spectroscopy. Longman, Harlow (1986).
14. N. Marchettini, Y. Yang and C. Rossi, J. Phys. Chem. 95, 10811 (1991).
15. E. O. Stejskal and J. E. Tanner, J. Chem. Phys. 42, 288 (1965).
16. R. A. Hoffman and S. Forsén, Prog. Nucl. Magn. Reson. Spectrosc. 1, 15 (1966).
17. J. H. Noggle, J. Magn. Reson. 35, 95 (1979).
18. C. Cativiela and F. Sánchez-Ferrando, Magn. Reson. Chem. 23, 1072 (1985).