Ferrimagnetic behavior of meso-tetrakis(2,3,5,6-tetrafluoro-4- methoxyphenyl)porphyrinatomanganese(III) tetracyanoethenide, [MnTF4OMePP][tcne] · 2 PhMe: Structural evidence for a second-order crystallographic phase transition

Chemistry - A European Journal

Volumn 5, Issue 6, 1999, Pages 1874-1881

  Rittenberg, Durrell K ^a   Sugiura, Ken Ichi ^b   Sakata, Yoshiteru ^b   Guzei, Ilia A ^c   Rheingold, Arnold L ^c   Miller, Joel S ^a  

^a UNIVERSITY OF UTAH   (United States)

^b OSAKA UNIVERSITY   (Japan)

^c UNIVERSITY OF DELAWARE   (United States)

Author keywords

Chain structures; Magnetic properties; Metalloporphryins; Phase transitions; Structure elucidation

Indexed keywords

FERROMAGNETIC MATERIAL; METALLOPORPHYRIN;

ARTICLE; CHEMICAL STRUCTURE; MAGNET; MAGNETISM; PHASE TRANSITION; STRUCTURE ANALYSIS; X RAY DIFFRACTION;

EID: 0033044892     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3765(19990604)5:6<1874::AID-CHEM1874>3.0.CO;2-2     Document Type: Article

References (60)

1. a) Proceedings of the Conference on Ferromagnetic and High Spin Molecular Based Materials, (Eds.: J. S. Miller, D. A. Dougherly), Mol. Cryst. Liq. Cryst. 1989, 176;
2. b) Proceedings of the Conference on Molecular Magnetic Materials, O. Kahn, D. Gatteschi, J. S. Miller, F. Palacio (Eds.);
3. c) NATO ARW Molecular Magnetic Materials. 1991, E1981;
4. d) Proceedings of the Conference on the Chemistry and Physics of Molecular Based Magnetic Materials, (Eds.: H. Iwamura, J. S. Miller), Mol. Cryst. Liq. Cryst. 1993, 232/233;
5. e) Proceedings of the Conference on Molecule-Based Magnets, (Eds.: J. S. Miller, A. J. Epstein), Mol. Cryst. Liq. Cryst. 1995, 271-274;
6. f) Proceedings of the Conference on Molecular-Based Magnets, (Eds.: K. Itoh, J. S. Miller, T. Takui), Mol. Cryst. Liq. Cryst. 1997, 305/306;
7. g) Molecular-based Magnetic Materials (Eds.: M. M. Turnbull, T. Sugimoto, L. K. Thompson). ACS Symposium Series No. 644. American Chemical Society, Washington, DC, 1996.
8. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
9. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
10. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
11. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
12. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
13. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
14. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
15. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
16. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
17. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
18. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
19. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
20. Reviews: a) A. L. Buchachenko, Russ. Chem. Rev. 1990, 59, 307; Usp. Khim. 1990, 59, 529: b) O. Kahn, Molecular Magnetism, VCH, New York, 1993; c) A. Caneschi, D. Gatteschi, R. Sessoli, P. Rey, Acc. Chem. Res. 1989, 22, 392; d) D. Gatteschi, Adv. Mater. 1994, 6, 635; e) J. S. Miller, A. J. Epstein, W. M. Reiff, Acc. Chem. Res. 1988, 21, 114; f) J. S. Miller, A. J. Epstein, W. M. Reiff, Science 1988, 240, 40 g) J. S. Miller, A. J. Epstein, W. M. Reiff, Chem. Rev. 1988, 88, 201; h) J. S. Miller, A. J. Epstein in New Aspects of Organic Chemistry, Vol. 237, (Eds.: Z. Yoshida, T. Shiba, Y. Ohsiro), VCH, New York, 1989; i) J. S. Miller, A. J. Epstein, Angew. Chem. 1994, 106, 399; Angew. Chem. Int. Ed. Engl. 1994, 33, 385; j) J. S. Miller, A. J. Epstein, Adv. Chem. Ser. 1995, 245, 161: k) J. S. Miller, A. J. Epstein, Chem. Eng. News 1995, 73(40), 30.
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32. b) K-i. Sugiura, A. Arif, D. K. Rittenberg, J. Schweizer, L. Öhrstrom, A. J. Epstein, J. S. Miller, Chem. Eur. J. 1997, 3, 138;
33. c) E. J. Brandon, K-i. Sugiura, A. M. Arif, L. Liable-Sands, A. L. Rheingold, J. S. Miller, Mol. Cryst. Liq. Cryst. 1997, 305, 269;
34. d) E. J. Brandon, B. M. Burkharl, R. D. Rogers, J. S. Miller, Chem. Eur. J. 1998, 4, 1938;
35. e) E. J. Brandon, D. K. Rittenberg, A. M. Arif, J. S. Miller, Inorg. Chem. 1998, 57, 3376;
36. f) E. J. Brandon, A. M. Arif, B. M. Burkhart, J. S. Miller, Inorg. Chem. 1998, 37, 2792.
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51. J. S. Miller, Adv. Mater. 1998, 10, 1553.
52. For example: a) J. Kirner, C. A. Reed, R. Scheldt, J. Am. Chem. Soc. 1977, 99, 1093; b) V. Day, R. Stultz, E. Tasset, R. Marianelli, Inorg. Nucl. Chem. Lett. 1975, 11, 505; c) R. Scheldt, K. Hatano, G. Rupprecht, P. Piciulo, Inorg. Chem. 1979, 18, 292.
53. For example: a) J. Kirner, C. A. Reed, R. Scheldt, J. Am. Chem. Soc. 1977, 99, 1093; b) V. Day, R. Stultz, E. Tasset, R. Marianelli, Inorg. Nucl. Chem. Lett. 1975, 11, 505; c) R. Scheldt, K. Hatano, G. Rupprecht, P. Piciulo, Inorg. Chem. 1979, 18, 292.
54. For example: a) J. Kirner, C. A. Reed, R. Scheldt, J. Am. Chem. Soc. 1977, 99, 1093; b) V. Day, R. Stultz, E. Tasset, R. Marianelli, Inorg. Nucl. Chem. Lett. 1975, 11, 505; c) R. Scheldt, K. Hatano, G. Rupprecht, P. Piciulo, Inorg. Chem. 1979, 18, 292.
55. B. M. Burkhart, B. G. Morin, A. J. Epstein, J. C. Calabrese, J. S. Miller, M. Sundaralingham, in press.
56. a) J. S. Miller, C. Vazquez, J. C. Calabrese, R. S. Mclean, A. J. Epstein, Adv. Mater. 1994, 6, 217;
57. b) J. S. Miller, C. Vazquez, N. Jones, L. R. S. McLean, A. Epstein, J. Mater. Chem. 1995, 5, 707.
58. J. Seiden, Phys. Lett. 1983, 44, L947.
59. C. M. Wynn, M. A. Girtu, K. I. Sugiura, E. J. Brandon, J. L. Manson, J. S. Miller, A. J. Epstein, Synth. Met. 1997, 85, 1695.
60. J. A. Mydosh, Spin Glassex. An Experimental Introduction, Taylor and Francis, London, 1993.