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In this reaction, even employing lower equivalents of tert-butylmagnesium chloride and AOC chloride did not give the N-mono-AOC derivative 13 or 15 as a major product.
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24
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85038154260
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When a methanol solution was used in this reaction, cleavage of the desired allylic protecting groups took place to some extent.
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25
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2-allyloxycarbonylation for obtaining an acceptable yield.
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