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For reviews on esterification, see: Ogliaruso, M.; Wolfe, J. F. The Chemistry of Functional Grou; Patai, S., Ed.; Wiley: Chichester; Suppl. B, Part 1, pp 411. Sutherland, I. O. Comprehensive Organic Chemistry; Barton, D. H. R.; Ollis, W. D., Ed.; Pergamon Press: Oxford, 1979; Vol. 2, pp 869. Sandler, S. R.; Karo, W. Organic Functional Group Preparations, Wasserman, H. H., Ed.; Academic Press: New York, 1983; Vol. 1, 2nd ed. pp 288. Mulzer, J. Comprehensive Organic Synthesis; Trost, B. M., Ed.; Pergamon Press: Oxford, 1991; Vol. 6, pp 323.
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Barton, D. H. R.; Ollis, W. D., Ed.; Pergamon Press: Oxford
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For reviews on esterification, see: Ogliaruso, M.; Wolfe, J. F. The Chemistry of Functional Grou; Patai, S., Ed.; Wiley: Chichester; Suppl. B, Part 1, pp 411. Sutherland, I. O. Comprehensive Organic Chemistry; Barton, D. H. R.; Ollis, W. D., Ed.; Pergamon Press: Oxford, 1979; Vol. 2, pp 869. Sandler, S. R.; Karo, W. Organic Functional Group Preparations, Wasserman, H. H., Ed.; Academic Press: New York, 1983; Vol. 1, 2nd ed. pp 288. Mulzer, J. Comprehensive Organic Synthesis; Trost, B. M., Ed.; Pergamon Press: Oxford, 1991; Vol. 6, pp 323.
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For reviews on esterification, see: Ogliaruso, M.; Wolfe, J. F. The Chemistry of Functional Grou; Patai, S., Ed.; Wiley: Chichester; Suppl. B, Part 1, pp 411. Sutherland, I. O. Comprehensive Organic Chemistry; Barton, D. H. R.; Ollis, W. D., Ed.; Pergamon Press: Oxford, 1979; Vol. 2, pp 869. Sandler, S. R.; Karo, W. Organic Functional Group Preparations, Wasserman, H. H., Ed.; Academic Press: New York, 1983; Vol. 1, 2nd ed. pp 288. Mulzer, J. Comprehensive Organic Synthesis; Trost, B. M., Ed.; Pergamon Press: Oxford, 1991; Vol. 6, pp 323.
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Though Kaminski et al. also reported the formation of DMTMM, its ability as a condensing agent was found to be poor, probably due to decomposition of DMTMM by demethylation giving 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)morpholine either before or during the reaction, see: ref 2, and Kaminski, Z. J.; Paneth, P.; Rudzinski, J. J. Org. Chem. 1998, 63, 4248.
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