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The crystals were obtained from chloroform by slow cooling from 60 °C in sealed vials. For each compound, at least five single crystals were tested. Under this crystallization condition, only one allotrope was found for each compound. No polymorphism was observed for this series of compounds. The X-ray data of 1c-g are given in the Supporting Information.
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(a) The layered packing of these compounds is also somewhat similar to the packing of some 4,4′-disubstituted meso hydrobenzoins. However, 4,4′-disubstituted meso hydrobenzoins examined mostly packed into different space groups and none crystalized into a noncentrosymmetric space group.
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