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1H NMR and UV-vis absorption spectrometry. Based on NMR analysis all dyes are > 97 % in the all-E-configuration. Satisfactory CHN analyses were obtained for 4, 5-7, 8a, 9b, 18, and 20b. Dyes 8b, 9a, 10, and 11, were characterized by mass spectrometry. Uncorrected melting points for 4: 200°C, 5: 216°C, 6: 259°C, 7: > 300°C, 8a: 225°C, 8b: 248°C, 9a: 185°C, 9b: 260°C, 10:250°C, 11: > 300°C, 18:102°C, 20b: 269°C.
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