Synthesis of submicron polycrystalline MFI zeolite films on porous ceramic supports

Journal of Membrane Science

Volumn 148, Issue 2, 1998, Pages 233-241

  Dong, Junhang ^a   Wegner, Karsten ^a   Lin, Y S ^a  

^a 705 Engineering Research Center   (United States)

Author keywords

Gas and vapor permeation; Gas permeation; Inorganic membranes; Membrane preparation and structure; Microporous and porous membranes; Silicalite; Submicron films; Yttria doped zirconia; Zeolite membranes

Indexed keywords

ALUMINA; CRYSTAL DEFECTS; FILM GROWTH; MASS TRANSFER; POLYCRYSTALLINE MATERIALS; POROSITY; SOL-GELS; SYNTHESIS (CHEMICAL); ULTRATHIN FILMS; YTTRIUM COMPOUNDS; ZEOLITES; ZIRCONIA;

INORGANIC MEMBRANES; SILICALITE; YTTRIA-DOPED ZIRCONIA;

GAS PERMEABLE MEMBRANES;

ALUMINUM OXIDE; OXYGEN; YTTRIUM; ZEOLITE; ZIRCONIUM OXIDE;

ARTICLE; CERAMICS; CONTROLLED STUDY; CRYSTAL; FILM; MEMBRANE STRUCTURE; PRIORITY JOURNAL; SYNTHESIS; THICKNESS;

EID: 0032582108     PISSN: 03767388     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0376-7388(98)00175-6     Document Type: Article

References (24)

1. Jia M., Chen B., Noble R.D., Falconer J. Ceramic-zeolite composite membranes and their application for separation of vapor/gas mixtures. J. Membr. Sci. 90:1994;1.
2. 3. Ind. Eng. Chem. Res. 34:1995;1652.
3. Y.H. Ma, S. Xiang, Formation of zeolite membranes from sols, US Patent 9 302 384 (1993).
4. Vroon Z.A.E.P., Keizer K., Gilde M.J., Verweij H., Burggraaf A.J. Transport properties of alkanes through ceramic thin zeolite MFI membranes. J. Membr. Sci. 113:1996;293.
5. Geus E.R., den Exter M.J., van Bekkum H. Synthesis and characterization of zeolite (MFI) membranes on porous ceramic supports. J. Chem. Soc., Faraday Trans. 88:1992;3101.
6. Sano T., Yanagishita H., Kiyozumi Y., Mizukami F., Haraya K. Separation of ethanol/water mixture by silicalite membrane on pervaporation. J. Membr. Sci. 95:1994;221.
7. Lovallo M.C., Tsapatsis M. Preferentially oriented submicron silicalite membranes. AIChE J. 42:1996;3020.
8. Schoeman B.J., Erdem-Senatalar A., Hedlund J., Sterte J. The growth of sub-micron films of TPA-silicalite-1 on single crystal silicon wafers from low-temperature clear solutions. Zeolites. 19:1997;21.
9. Yan Y., Davis M.E., Gavalas G.R. Preparation of highly selective zeolite ZSM-5 membranes by a post-synthetic coking treatment. J. Membr. Sci. 123:1997;95.
10. Bai C., Jia M., Falconer J.L., Noble R.D. Preparation and separation properties of silicalite composite membranes. J. Membr. Sci. 105:1995;79.
11. Sano T., Ejiri S., Yamada K., Kawakami Y., Yanagishita H. Separation of acetic-water mixtures by pervaporation through silicalite membrane. J. Membr. Sci. 123:1997;225.
12. Kim J., Lin Y.S. Sol-gel synthesis and characterization of yttria stabilized zirconina membranes. J. Membr. Sci. 193:1998;75.
13. Gopalan R., Chang C.-H., Lin Y.S. Thermal stability improvement on pore and phase structure of sol-gel derived zirconia. J. Mater. Sci. 30:1995;3075.
14. Geus E.R., van Bekkum H. Calcination of large MFI-type single crystals, Part 2: Crack formation and thermomechanical properties in view of the preparation of zeolite membranes. Zeolites. 15:1995;333.
15. den Exter M.J., van Bekkum H., Rijn C.J.M., Kapteijn F., Moulijn J.A., Schellevis H., Beenakker C.I.N. Stability of oriented silicalite-1 films in view of zeolite membrane preparation. Zeolites. 19:1997;13.
16. Treacy M.M.J., Higgins J.B., von Ballmoos R. Collection of simulated XRD powder patterns for zeolites: powder pattern identification tables. Zeolites. 16:1996;323.
17. Y.S. Lin, Ph.D. Thesis, University of Twente, The Netherlands, 1992.
18. M.J. den Exter, J.C. Jansen, J.M. van de Graaf, F. Kapteijn, J.A. Moulijn, H. van Bekkum, Zeolite-based membranes preparation, performance and prospects, in: H. Chon, S.I. Woo, S.-E. Park (Eds.), Recent Advances and New Horizons in Zeolite Science and Technology, Stud. Surf. Sci. Catal. 102 (1996) 413.
19. V. Valtchev, S. Mintova, I. Vasilev, The effect of plastic deformation and thermal annealing of the copper substrate on the zeolite film formation, J. Chem. Soc., Chem. Commun. (1994) 979.
20. Davis S.P., Borgstedt E.V.R., Suib S.L. Growth of zeolite crystallites and coatings on metal surface. Chem. Mater. 2:1990;712.
21. Jia M., Peinemann K.-V., Behling R.D. Ceramic zeolite composite membranes. Preparation, characterization and gas permeation. J. Membr. Sci. 82:1993;15.
22. Coronas J., Falconer J.L., Noble R.D. Characterization and permeation properties of ZSM-5 tubular membranes. AIChE J. 43:1997;1797.
23. Bakker W.J.W., Kapteijn F., Poppe J., Moulijn J.A. Permeation characteristics of a metal-supported silicalite-1 zeolite membrane. J. Membr. Sci. 117:1996;57.
24. Bakker W.J.W., van den Broeke L.J.P., Kapteijn F., Moulijn J.A. Temperature dependence of one-component permeation through a silicalite-1 membrane. AIChE J. 43:1997;2203.