Measurement and control of interface strength of RF magnetron-sputtered Ca-PO coatings on Ti-6A1-4V substrates using a laser spallation technique

Journal of Biomedical Materials Research

Volumn 41, Issue 4, 1998, Pages 624-632

  Van Dijk, K ^a   Gupta, V ^b   Yu, A K ^b   Jansen, J A ^a  

^a RADBOUD UNIVERSITY NIJMEGEN   (Netherlands)

^b UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

Calcium phosphate coatings; Interface strength; RF magnetron sputter deposition

Indexed keywords

CALCIUM COMPOUNDS; COATINGS; INTERFACES (MATERIALS); LASER APPLICATIONS; MAGNETRON SPUTTERING; MECHANICAL VARIABLES MEASUREMENT; NEODYMIUM LASERS; SCANNING ELECTRON MICROSCOPY; SPALLING; TENSILE STRENGTH; TITANIUM ALLOYS;

CALCIUM PHOSPHATE COATINGS; INTERFACE STRENGTH; LASER SPALLATION; MAGNETRON SPUTTER DEPOSITION; TITANIUM ALUMINUM ALLOY;

IMPLANTS (SURGICAL);

CALCIUM PHOSPHATE; TITANIUM;

BIOCOMPATIBILITY; BONE PROSTHESIS; CONFERENCE PAPER; FILM; LASER; MECHANICAL STRESS; METAL IMPLANTATION; OXYGEN TENSION; PHYSICAL CHEMISTRY; PROSTHESIS MATERIAL; SURFACE PROPERTY; TENSILE STRENGTH;

CALCIUM PHOSPHATES; LASERS; MAGNETICS; MATERIALS TESTING; MICROSCOPY, ELECTRON, SCANNING; TENSILE STRENGTH; TITANIUM;

EID: 0032531284     PISSN: 00219304     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-4636(19980915)41:4<624::AID-JBM15>3.0.CO;2-E     Document Type: Conference Paper

References (38)

1. H. Caulier, J. P. C. M. van der Waerden, Y. C. G. J. Paquay, J. G. C. Wolke, W. Kalk, I. Naert, and J. A. Jansen, "Effect of calcium phosphate (Ca-P) coatings on trabecular bone response: A histological study," J. Biomed. Mater. Res., 29, 1061-1069 (1995).
2. C. P. A. T. Klein, P. Patka, J. G. C. Wolke, J. M. A. de Blieck-Hogervorst, and K. de Groot, "Long-term in vivo study of plasma-sprayed coatings on titanium alloys of tetracalcium phosphate, hydroxyapatite, and a-tricalcium phosphate," Biomaterials, 15, 146-150 (1994).
3. K. Seballe, "Hydroxyapatite ceramic coating for bone implant fixation," Acta Scand., S255 (1993).
4. W. J. A. Dhert, C. P. A. T. Klein, J. A. Jansen, E. A. van der Velde, R. C. Vriesde, P. M. Rozing, and K. de Groot, "A histological and histomorphometrical investigational fluoraparite, magnesium whitlockite, and hydroxyapatite plasma-sprayed coatings in goats," J. Biomed. Mater. Res., 27, 127-138 (1993).
5. M. Gottlander, T. Albrektsson, and L. V. Carlsson, "A histomorphometric study of unthreaded hydroxyapatite-coated and titanium-coated implants in rabbit bone," Int. J. Oral Maxillofac. Impl., 7, 485-490 (1992).
6. J. L. Ong, L. A. Harris, L. C. Lucas, W. R. Lacefield, and D. Rigney, "Structure, solubility and bond strength of thin calcium phosphate coatings produced by ion-beam sputter deposition," Biomaterials, 13, 249-254 (1992).
7. A. M. Ektessabi, "Ion beam processing of bio-ceramics," Nucl. Instr. and Meth. Phys. Res. B, 99, 610-613 (1995).
8. C. M. Cotell, "Pulsed laser deposition and processing of biocompatible hydroxylapatite thin films," Appl. Surf. Sci., 69, 140-148 (1993).
9. M. Jelinek, V. Olšan, L. Jastrabík, V. Studnička, V. Hnatowicz, J. Kvítek, V. Havránek, T. Dostálová, I. Zergioti, A. Petrakis, E. Hontzopoulos, and C. Fotakis, "Effect of processing parameters on the properties of hydroxylapatite films grown by pulsed laser deposition," Thin Solid Films, 257, 125-129 (1995).
10. J. A. Jansen, J. C. G. Wolke, S. Swann, J. P. C. M. van der Waerden, and K. de Groot, "Application of magnetron sputtering for producing ceramic coatings on implant materials," Clin. Oral Impl. Res., 4, 28-34 (1993).
11. J. G. C. Wolke, K. van Dijk, H. G. Schaeken, K. de Groot, and J. A. Jansen, "A study of the surface characteristics of magnetron sputter calcium phosphate coatings," J. Biomed. Mater. Res., 26, 1477-1484 (1994).
12. K. van Dijk, H. G. Schaeken, J. G. C. Wolke, C. H. M. Marée, F. H. P. M. Habraken, J. Verhoeven, and J. A. Jansen, "Influence of discharge power level on the properties of hydroxyapatite films deposited on Ti6A14V with rf magnetron sputtering," J. Biomed. Mater. Res., 29, 269-276 (1995).
13. K. van Dijk, H. G. Schaeken, J. G. C. Wolke, and J. A. Jansen, "Influence of annealing temperature on RF magnetron sputtered calcium phosphate coatings," Biomaterials, 17, 405-410 (1996).
14. J. E. G. Hulshoff, K. van Dijk, J. P. C. M. van der Waerden, J. G. C. Wolke, L. A. Ginsel, and J. A. Jansen, "Biological evaluation of the effect of magnetron-sputtered Ca/P coatings on bone behavior in vitro," J. Biomed. Mater. Res., 29, 967-975 (1995).
15. 3OH layers," Surf. Coat. Technol., 76-77, 206-210 (1995).
16. 3OH target," Thin Solid Films, to appear.
17. J. E. G. Hulshoff, K. van Dijk, J. E. de Ruijter, F. J. R. Rietveld, L. A. Ginsel, and J. A. Jansen, "Interfacial phenomena: An in vitro study of the effect of calcium phosphate (Ca-P) ceramic on bone formation," J. Biomed. Mater Res., 40, 464-474 (1998).
18. V. Gupta, J. Yuan, and D. Martinez, "Calculation, measurement and control of interface strength in composites," J. Am. Ceram. Soc., 76, 305-315 (1993).
19. y. hard coatings," Surf. Coat. Technol., 60, 428-433 (1993).
20. M. K. Puchert, P. Y. Timbrell, and R. N. Lamb, "Thickness-dependent stress in sputtered carbon films," J. Vac. Sci. Technol. A, 12 (3), 727-732 (1994).
21. V. Gupta and J. Yuan, "Measurement of interface strength by the modified laser spallation technique. II. Applications to metal/ceramic interfaces," J. Appl Phys., 74 (4), 2397-2404 (1993).
22. C.-J. Lu, and D. B. Bogy, "The effect of tip radius on nano-indentation hardness tests," Int. J Solids Struc., 32 (12), 1770-1795 (1995).
23. J. Yuan and V. Gupta, "Measurement of interface strength by the modified laser spallation technique. I. Experiment and simulation of the spallation process," J. Appl. Phys., 74 (4), 2388-2396 (1993).
24. V. Gupta, J. Yuan, and A. Pronin, "Recent developments in the laser spallation technique to measure the interface strength and its relationship to interface toughness with applications to metal/ceramic, ceramic/ceramic and ceramic/polymer interfaces," J. Adhesion Sci. Technol., 8 (6), 713-747 (1994).
25. V. Gupta, J. Yuan, and A. Pronin, "Nanosecond rise time laser produced stress pulses with no asymptotic decay," Rev. Sci. Instrum., 64 (6), 1611-1613 (1993).
26. V. Gupta, J. Wu, and A. N. Pronin, "Effect of substrate orientation and deposition mode on the tensile strength and toughness of Nb/sapphire interfaces," J. Am. Ceram. Soc., to appear.
27. A. S. Argon, J. A. Cornie, V. Gupta, L. Lev, and D. M. Parks, "Response to the comments of Nutt and King on the bond strength measurements," Mater. Sci. Eng., to appear.
28. Jun Yuna, Measurement of Interface Strength. Interface Fracture Mechanisms and Their Dependence on Microstructure and Chemistry, Ph.D. Thesis, Thayer School of Engineering, Dartmouth College, Hanover, New Hampshire, 1994.
29. J. Yuan and V. Gupta, "The effect of microstructure and chemistry on the tensile strength of Nb/sapphire interfaces, with and without the interlayers of Cr and Sb," Acta Metal. Mater., 43 (2), 781-794 (1995).
30. J. Yuan, V. Gupta, and M. Kim, "Structure and chemistry of Nb/sapphire interfaces, with and without the interlayers of Sb and Cr," Acta Metal Mater., 43 (2), 769-779 (1995).
31. V. Gupta and A. Pronin, "A new technique to measure the toughness of thin film interfaces," J. Am. Ceram. Soc., 78 (5), 1397-1400 (1995).
32. W. K. Chu, J. W. Mayer, and M.-A. Nicolet, Backscattering Spectrometry, Academic Press, Inc., New York, 1978.
33. K. T. Scott, in Ceramic Surfaces and Surface Treatments, British Ceramic Society, Shelton, 1984, p. 195
34. M. J. Filiaggi and R. M. Pilliar, "Mechanical testing of plasma-sprayed ceramic coatings on metal substrates: Interfacial fracture toughness and tensile bond strength," J. Mater. Sci., 26, 5383-5395 (1991).
35. K. L. Chopra, "Mechanical effects in thin films," in Thin Film Phenomena, McGraw-Hill, New York.
36. K. L. Chopra, Ledgemont Laboratory Report, June 1968.
37. B. N. Chapman, J. Vac. Sci. Technol., 11, 109 (1974).
38. I. M. O Kangasniemi, C. C. P. M. Verheyen, E. A. van der Velde, and K. de Groot, "In vivo tensile testing of flourapatite and hydroxylapatite plasma-sprayed coatings," J. Biomed. Mater. Res., 28, 563-572 (1994).