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27Al NMR spectrum of 2 did not contain any signals.
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32
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0344500231
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note
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[21] The structure was refined as a racemic twin. b) Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101096. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223336-033; e-mail: deposit@ccdc.cam.ac.uk).
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