Synthesis and structural analysis of a helical coordination polymer formed by the self-assembly of a 2,2'-bipyridine-based exo-ditopic macrocyclic ligand and silver cations

Angewandte Chemie - International Edition

Volumn 37, Issue 7, 1998, Pages 920-922

  Kaes, Christian ^a   Hosseini, Mir Wais ^a   Rickard, Clifton E F ^b   Skelton, Brian W ^c   White, Allan H ^c  

^a UNIVERSITÉ DE STRASBOURG   (France)

^b UNIVERSITY OF AUCKLAND   (New Zealand)

^c UNIVERSITY OF WESTERN AUSTRALIA   (Australia)

Author keywords

Coordination polymers; Helical structures; N ligands; Self assembly; Silver

Indexed keywords

EID: 0031971663     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3773(19980420)37:7<920::AID-ANIE920>3.0.CO;2-O     Document Type: Article

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39. max, = 0.351 0.86 (SADABS), Xtal 3.4 program system. Phenyl and pyridine rings were refined as rigid bodies, and the geometries of the anions and solvent molecules were constrained to "idealized" values, with isotropic thermal parameters. Ring 24n was modeled as disordered over two sets of sites of equal occupancy. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC-100747. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).