-
3
-
-
0000178635
-
-
Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson, Pergamon, NY
-
b) S. G. Davies, T. D. McCarthy, in Comprehensive Organometallic Chemistry II, Vol. 12 (Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson), Pergamon, NY, 1995, pp. 1039-1070;
-
(1995)
Comprehensive Organometallic Chemistry II
, vol.12
, pp. 1039-1070
-
-
Davies, S.G.1
McCarthy, T.D.2
-
4
-
-
0000958965
-
-
Ed.: L. S. Liebeskind, JAI, London
-
c) M. Uemura, in Advances in Metal Organic Chemistry, Vol. 2 (Ed.: L. S. Liebeskind), JAI, London, 1989, pp. 195-245.
-
(1989)
Advances in Metal Organic Chemistry
, vol.2
, pp. 195-245
-
-
Uemura, M.1
-
6
-
-
0030964985
-
-
b) A. Quattropani, G. Anderson, G. Bernardinelli, E. P. Kündig, J. Am. Chem. Soc. 1997, 119, 4773;
-
(1997)
J. Am. Chem. Soc.
, vol.119
, pp. 4773
-
-
Quattropani, A.1
Anderson, G.2
Bernardinelli, G.3
Kündig, E.P.4
-
7
-
-
0000575353
-
-
c) M. Brands, H. G. Wey, J. Bruckmann, C. Krüger, H. Butenschön, Chem. Eur. J. 1996, 2, 182;
-
(1996)
Chem. Eur. J.
, vol.2
, pp. 182
-
-
Brands, M.1
Wey, H.G.2
Bruckmann, J.3
Krüger, C.4
Butenschön, H.5
-
8
-
-
0001492945
-
-
d) K. Kamikawa, T. Watanabe, M. Uemura, J. Org. Chem. 1996, 61, 1375.
-
(1996)
J. Org. Chem.
, vol.61
, pp. 1375
-
-
Kamikawa, K.1
Watanabe, T.2
Uemura, M.3
-
10
-
-
0002933593
-
-
Ed.: L. S. Liebeskind, JAI, London
-
a) A. Solladié-Cavallo, in Advances in Metal Organic Chemistry, Vol. 2 (Ed.: L. S. Liebeskind), JAI, London, 1989, pp. 99-133;
-
(1989)
Advances in Metal Organic Chemistry
, vol.2
, pp. 99-133
-
-
Solladié-Cavallo, A.1
-
11
-
-
0010617428
-
-
Eds.: H. Werner, G. Erker, Springer, Berlin, Heidelberg
-
b) K. Schlögl, in Organometallics in Organic Synthesis 2 (Eds.: H. Werner, G. Erker), Springer, Berlin, Heidelberg, 1989, pp. 63-77.
-
(1989)
Organometallics in Organic Synthesis
, vol.2
, pp. 63-77
-
-
Schlögl, K.1
-
12
-
-
0345195328
-
-
a) C. Mukai, I. J. Kim, M. Hanaoka, Tetrahedron Lett. 1993, 34, 681;
-
(1993)
Tetrahedron Lett.
, vol.34
, pp. 681
-
-
Mukai, C.1
Kim, I.J.2
Hanaoka, M.3
-
13
-
-
0027305932
-
-
b) C. Mukai, I. J. Kim, E. Furu, M. Hanaoka, Tetrahedron 1993, 49, 8323;
-
(1993)
Tetrahedron
, vol.49
, pp. 8323
-
-
Mukai, C.1
Kim, I.J.2
Furu, E.3
Hanaoka, M.4
-
16
-
-
0027527644
-
-
a) H.-G. Schmalz, J. Hollander, M. Arnold, G. Dürner, Tetrahedron Lett. 1993, 34, 6259;
-
(1993)
Tetrahedron Lett.
, vol.34
, pp. 6259
-
-
Schmalz, H.-G.1
Hollander, J.2
Arnold, M.3
Dürner, G.4
-
17
-
-
0002486371
-
-
b) H.-G. Schmalz, M. Arnold, J. Hollander, J. W. Bats, Angew. Chem. 1994, 106, 77; Angew. Chem. Int. Ed. Engl. 1994, 33, 109;
-
(1994)
Angew. Chem.
, vol.106
, pp. 77
-
-
Schmalz, H.-G.1
Arnold, M.2
Hollander, J.3
Bats, J.W.4
-
18
-
-
33748242413
-
-
b) H.-G. Schmalz, M. Arnold, J. Hollander, J. W. Bats, Angew. Chem. 1994, 106, 77; Angew. Chem. Int. Ed. Engl. 1994, 33, 109;
-
(1994)
Angew. Chem. Int. Ed. Engl.
, vol.33
, pp. 109
-
-
-
19
-
-
0027991269
-
-
c) H.-G. Schmalz, A. Schwarz, G. Dürner, Tetrahedron Lett. 1994, 35, 6861;
-
(1994)
Tetrahedron Lett.
, vol.35
, pp. 6861
-
-
Schmalz, H.-G.1
Schwarz, A.2
Dürner, G.3
-
20
-
-
0029059563
-
-
d) H.-G. Schmalz, A. Majdalani, T. Geller, J. Hollander, J. W. Bats, ibid. 1995, 36, 4777;
-
(1995)
Tetrahedron Lett.
, vol.36
, pp. 4777
-
-
Schmalz, H.-G.1
Majdalani, A.2
Geller, T.3
Hollander, J.4
Bats, J.W.5
-
21
-
-
0030005806
-
-
e) H.-G. Schmalz, S. Siegel, A. Schwarz, ibid. 1996, 37, 2947;
-
(1996)
Tetrahedron Lett.
, vol.37
, pp. 2947
-
-
Schmalz, H.-G.1
Siegel, S.2
Schwarz, A.3
-
23
-
-
0019840547
-
-
G. C. Harbour, A. A. Thymiak, K. L. Rinehart, Jr., P. D. Shaw, R. G. Hughes, Jr., S. A. Mizsak, J. H. Coats, G. E. Zurenko, L. H. Li, S. L. Kuentzel, J. Am. Chem. Soc. 1981, 103, 5604.
-
(1981)
J. Am. Chem. Soc.
, vol.103
, pp. 5604
-
-
Harbour, G.C.1
Thymiak, A.A.2
Rinehart Jr., K.L.3
Shaw, P.D.4
Hughes Jr., R.G.5
Mizsak, S.A.6
Coats, J.H.7
Zurenko, G.E.8
Li, L.H.9
Kuentzel, S.L.10
-
24
-
-
0344764837
-
-
mention a crystal structure of 1 which, however, has never been published
-
Harbour et al. (ref. [8]) mention a crystal structure of 1 which, however, has never been published.
-
J. Am. Chem. Soc.
-
-
Harbour1
-
29
-
-
0025348431
-
-
M. Asaoka, M. Sakurai, H. Takei, Tetrahedron Lett. 1990, 31, 4759.
-
(1990)
Tetrahedron Lett.
, vol.31
, pp. 4759
-
-
Asaoka, M.1
Sakurai, M.2
Takei, H.3
-
30
-
-
0022871021
-
-
a) T. Uyehara, T. Furuta, Y. Kabasawa, J. Yamada, T. Kato, J. Chem. Soc. Chem. Commun. 1986, 539;
-
(1986)
J. Chem. Soc. Chem. Commun.
, pp. 539
-
-
Uyehara, T.1
Furuta, T.2
Kabasawa, Y.3
Yamada, J.4
Kato, T.5
-
31
-
-
33845277881
-
-
b) T. Uyehara, T. Furuta, Y. Kabasawa, J. Yamada, T. Kato, Y. Yamamoto, J. Org. Chem. 1988, 53, 3669.
-
(1988)
J. Org. Chem.
, vol.53
, pp. 3669
-
-
Uyehara, T.1
Furuta, T.2
Kabasawa, Y.3
Yamada, J.4
Kato, T.5
Yamamoto, Y.6
-
34
-
-
0029125236
-
-
R. Tavares, D. Daloze, J. C. Braekman, E. Hajdu, R. W. M. Van Soest, J. Nat. Prod. 1995, 58, 1139.
-
(1995)
J. Nat. Prod.
, vol.58
, pp. 1139
-
-
Tavares, R.1
Daloze, D.2
Braekman, J.C.3
Hajdu, E.4
Van Soest, R.W.M.5
-
35
-
-
0013587192
-
-
R. A. Barrow, L. M. Murray, T. K. Lim, R. J. Capon, Aust. J. Chem. 1996, 49, 767.
-
(1996)
Aust. J. Chem.
, vol.49
, pp. 767
-
-
Barrow, R.A.1
Murray, L.M.2
Lim, T.K.3
Capon, R.J.4
-
36
-
-
0012192213
-
-
Parts of this work were communicated in a preliminary form: a) H.-G. Schmalz, K. Schellhaas, Angew. Chem. 1996, 108, 2277; Angew. Chem. Int. Ed. Engl. 1996, 35, 2146;
-
(1996)
Angew. Chem.
, vol.108
, pp. 2277
-
-
Schmalz, H.-G.1
Schellhaas, K.2
-
37
-
-
0029821411
-
-
Parts of this work were communicated in a preliminary form: a) H.-G. Schmalz, K. Schellhaas, Angew. Chem. 1996, 108, 2277; Angew. Chem. Int. Ed. Engl. 1996, 35, 2146;
-
(1996)
Angew. Chem. Int. Ed. Engl.
, vol.35
, pp. 2146
-
-
-
39
-
-
0000900750
-
-
Eds.: B. M. Trost, I. Fleming, Pergamon, Oxford
-
For reviews on nucleophilic additions to arene complexes, see: a) M. F. Semmelhack, in Comprehensive Organic Synthesis. Vol. 4 (Eds.: B. M. Trost, I. Fleming), Pergamon, Oxford, 1991, p. 517;
-
(1991)
Comprehensive Organic Synthesis
, vol.4
, pp. 517
-
-
Semmelhack, M.F.1
-
40
-
-
0000747080
-
-
Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson, Pergamon, NY
-
b) M. F. Semmelhack, in Comprehensive Organometallic Chemistry II, Vol. 12 (Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson), Pergamon, NY, 1995, p. 979.
-
(1995)
Comprehensive Organometallic Chemistry II
, vol.12
, pp. 979
-
-
Semmelhack, M.F.1
-
41
-
-
33845559129
-
-
a) M. F. Semmelhack, J. Bisaha, M. Czarny, J. Am. Chem. Soc. 1979, 101, 768;
-
(1979)
J. Am. Chem. Soc.
, vol.101
, pp. 768
-
-
Semmelhack, M.F.1
Bisaha, J.2
Czarny, M.3
-
44
-
-
0000747083
-
-
Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson, Pergamon, NY
-
d) for a review, see: M. F. Semmelhack, in Comprehensive Organometallic Chemistry II, Vol. 12 (Eds.: E. W. Abel, F. G. A. Stone, G. Wilkinson), Pergamon, NY, 1995, p. 1017.
-
(1995)
Comprehensive Organometallic Chemistry II
, vol.12
, pp. 1017
-
-
Semmelhack, M.F.1
-
45
-
-
0000160409
-
-
a) D. A. Price, N. S. Simpkins, A. M. MacLeod, A. P. Watt, J. Org. Chem. 1994, 59, 1961:
-
(1994)
J. Org. Chem.
, vol.59
, pp. 1961
-
-
Price, D.A.1
Simpkins, N.S.2
MacLeod, A.M.3
Watt, A.P.4
-
48
-
-
33748668254
-
-
d) R. A. Ewin, A. M. MacLeod, D. A. Price, N. S. Simpkins, A. P. Watt, J. Chem. Soc. Perkin Trans. 1 1997, 401-415;
-
(1997)
J. Chem. Soc. Perkin Trans. 1
, pp. 401-415
-
-
Ewin, R.A.1
MacLeod, A.M.2
Price, D.A.3
Simpkins, N.S.4
Watt, A.P.5
-
50
-
-
0000208914
-
-
a) M. F. Semmelhack, J. J. Harrison, Y. Thebtaranonth, J. Org. Chem. 1979, 44, 3275;
-
(1979)
J. Org. Chem.
, vol.44
, pp. 3275
-
-
Semmelhack, M.F.1
Harrison, J.J.2
Thebtaranonth, Y.3
-
51
-
-
33845559718
-
-
b) M. F. Semmelhack, H. T. Hall, Jr., R. Farina, M. Yoshifuji, G. Clark, T. Bargar, K. Hirotsu, J. Clardy, J. Am. Chem. Soc. 1979, 101, 3535;
-
(1979)
J. Am. Chem. Soc.
, vol.101
, pp. 3535
-
-
Semmelhack, M.F.1
Hall Jr., H.T.2
Farina, R.3
Yoshifuji, M.4
Clark, G.5
Bargar, T.6
Hirotsu, K.7
Clardy, J.8
-
52
-
-
0008583009
-
-
c) M. F. Semmelhack, G. R. Clark, J. L. Garcia, J. J. Harrison, Y. Thebtaranonth, W. Wulff, A. Yamashita, Tetrahedron 1981, 37, 3957.
-
(1981)
Tetrahedron
, vol.37
, pp. 3957
-
-
Semmelhack, M.F.1
Clark, G.R.2
Garcia, J.L.3
Harrison, J.J.4
Thebtaranonth, Y.5
Wulff, W.6
Yamashita, A.7
-
54
-
-
0011048651
-
-
a) R. C. Cambie, P. S. Rutledge, R. J. Stevenson, P. D. Woodgate, J. Organomet. Chem. 1995, 486, 199;
-
(1995)
J. Organomet. Chem.
, vol.486
, pp. 199
-
-
Cambie, R.C.1
Rutledge, P.S.2
Stevenson, R.J.3
Woodgate, P.D.4
-
55
-
-
0030964985
-
-
for a recent report on a related cyclohexenone formation involving nucleophile addition to ent-7, see: b) A. Quattropani, G. Anderson, G. Bernardinelli, E. P. Kündig, J. Am. Chem. Soc. 1997, 119, 4773.
-
(1997)
J. Am. Chem. Soc.
, vol.119
, pp. 4773
-
-
Quattropani, A.1
Anderson, G.2
Bernardinelli, G.3
Kündig, E.P.4
-
57
-
-
0030008278
-
-
b) A. J. Pearson, A. V. Gontcharov, P. D. Woodgate, Tetrahedron Lett. 1996, 37, 3087.
-
(1996)
Tetrahedron Lett.
, vol.37
, pp. 3087
-
-
Pearson, A.J.1
Gontcharov, A.V.2
Woodgate, P.D.3
-
59
-
-
33947480171
-
-
3) which in turn was prepared from (S)-(-)-phenylethylamine (Fluka) following the procedure of Overberger et al.: C. G. Overberger, N. P. Marullo, R. G. Hiskey, J. Am. Chem. Soc. 1961, 83, 1374. The enantiomeric purity of (S,S)-di(1-phenylethyl)amine (≥99% ee) was confirmed by chiral HPLC (Daicel, Chiralcel OJ, hexane/2-propanol = 9:1).
-
(1961)
J. Am. Chem. Soc.
, vol.83
, pp. 1374
-
-
Overberger, C.G.1
Marullo, N.P.2
Hiskey, R.G.3
-
60
-
-
0344764821
-
-
note
-
A 25 m fused silica column modified with heptakis(6-O-TBDMS-2,3-di-O-methyl)-β-cyclodextrin (50% in OV 1701) was found to be suitable for the separation of rac-7 by Prof. W. A. König, University of Hamburg, Germany. We thank Prof. König for providing us with such a column.
-
-
-
-
62
-
-
33845559129
-
-
for a different procedure for the preparation of rac-14, see: b) M. F. Semmelhack, J. Bisaha, M. Czarny, J. Am. Chem. Soc. 1979, 101, 768.
-
(1979)
J. Am. Chem. Soc.
, vol.101
, pp. 768
-
-
Semmelhack, M.F.1
Bisaha, J.2
Czarny, M.3
-
63
-
-
0001466430
-
-
a) E. J. Corey, D. Seebach, Angew. Chem. 1965, 77, 1134, 1135; Angew. Chem. Int. Ed. Engl. 1965, 4, 1075, 1077;
-
(1965)
Angew. Chem.
, vol.77
, pp. 1134
-
-
Corey, E.J.1
Seebach, D.2
-
64
-
-
33748737077
-
-
a) E. J. Corey, D. Seebach, Angew. Chem. 1965, 77, 1134, 1135; Angew. Chem. Int. Ed. Engl. 1965, 4, 1075, 1077;
-
(1965)
Angew. Chem. Int. Ed. Engl.
, vol.4
, pp. 1075
-
-
-
66
-
-
0005262595
-
-
Technische Universität Berlin
-
For details, see: a) N. Strack, Diplomarbeit, Technische Universität Berlin 1996;
-
(1996)
Diplomarbeit
-
-
Strack, N.1
-
68
-
-
0345195315
-
-
note
-
1H NMR analysis of the product mixture indicated rac16 (R = Me) as the major component.
-
-
-
-
70
-
-
0344764817
-
-
note
-
-3.
-
-
-
-
71
-
-
0345195313
-
-
note
-
The enantiomeric analysis was performed with HPLC on a Daicel Chiralcel OJ column. The separation conditions were optimized using racemic samples.
-
-
-
-
79
-
-
0019840547
-
-
Here we apply the numbering system for ptilocaulin introduced by Rinehart (ref. [8]).
-
(1981)
J. Am. Chem. Soc.
, vol.103
, pp. 5604
-
-
Harbour, G.C.1
Thymiak, A.A.2
Rinehart Jr., K.L.3
Shaw, P.D.4
Hughes Jr., R.G.5
Mizsak, S.A.6
Coats, J.H.7
Zurenko, G.E.8
Li, L.H.9
Kuentzel, S.L.10
-
80
-
-
0344764809
-
-
note
-
-3.
-
-
-
-
81
-
-
0345195310
-
-
note
-
-3.
-
-
-
-
82
-
-
0004312524
-
-
Verlag Helvetica Chimica Acta, Basel, ch. 15
-
a) G. Quinkert, E. Egert, C. Griesinger, Aspekte der Organischen Chemie, Verlag Helvetica Chimica Acta, Basel, 1995, ch. 15;
-
(1995)
Aspekte der Organischen Chemie
-
-
Quinkert, G.1
Egert, E.2
Griesinger, C.3
-
85
-
-
0039426508
-
-
methylguanidinium nitrate
-
The only crystal structures of guanidinium nitrates found in the Cambridge Structural Database are the following: a) R. M. Curtis, R. A. Pasternak, Acta Crystallogr. 1955, 8, 675 (methylguanidinium nitrate);
-
(1955)
Acta Crystallogr.
, vol.8
, pp. 675
-
-
Curtis, R.M.1
Pasternak, R.A.2
-
86
-
-
0001722871
-
-
diaminoguanidinium nitrate
-
b) J. P. Ritchie, K.-L. Lee, D. T. Cromer, E. M. Kober, D. D. Lee, J. Org. Chem. 1990, 55, 1994 (diaminoguanidinium nitrate);
-
(1990)
J. Org. Chem.
, vol.55
, pp. 1994
-
-
Ritchie, J.P.1
Lee, K.-L.2
Cromer, D.T.3
Kober, E.M.4
Lee, D.D.5
-
89
-
-
0030122704
-
-
biguanidinium dinitrate
-
e) A. Martin, A. A. Pinkerton, A. Schiemann, ibid. 1996, 52, 966 (biguanidinium dinitrate).
-
(1996)
Acta Crystallogr. Sect. C
, vol.52
, pp. 966
-
-
Martin, A.1
Pinkerton, A.A.2
Schiemann, A.3
-
91
-
-
0041045434
-
-
D. M. Daddwell, D. T. Pegg, M. R. Bendall, J. Magn. Reson. 1982, 48, 323.
-
(1982)
J. Magn. Reson.
, vol.48
, pp. 323
-
-
Daddwell, D.M.1
Pegg, D.T.2
Bendall, M.R.3
-
92
-
-
0002714675
-
-
W. C. Still, M. Kahn, A. Mitra, J. Org. Chem. 1978, 43, 2923.
-
(1978)
J. Org. Chem.
, vol.43
, pp. 2923
-
-
Still, W.C.1
Kahn, M.2
Mitra, A.3
-
93
-
-
0345627307
-
-
note
-
1H NMR analysis). In the case of 16 (R = Me), a single characteristic olefinic signal (m) at δ = 6.0 indicated the dominance of one double-bond isomer.
-
-
-
-
94
-
-
0345195307
-
-
note
-
2Si: C 59.95, H 8.29; found: C 59.80, H 8.36. The NMR data were identical to those reported for 18.
-
-
-
-
95
-
-
0345195305
-
-
We thank Dr. G. Zimmermann, University of Frankfurt/Main, for recording the NMR spectra of 1/23 on a Bruker AM 600 instrument
-
We thank Dr. G. Zimmermann, University of Frankfurt/Main, for recording the NMR spectra of 1/23 on a Bruker AM 600 instrument.
-
-
-
|