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Volumn 37, Issue 17, 1996, Pages 2947-2950

Radical cyclization of η6-arene-Cr(CO)3 complexes: A regio-and stereoselective entry to functionalized pseudopterosin precursors

Author keywords

[No Author keywords available]

Indexed keywords

ARENE;

EID: 0030005806     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00486-8     Document Type: Article
Times cited : (58)

References (45)
  • 6
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    • b) Schmalz, H.-G.; Arnold, M.; Hollander, J.; Bats, J.W. Angew. Chem. 1994, 106, 77; Angew. Chem. Int. Ed. Engl. 1994, 33, 109;
    • (1994) Angew. Chem. Int. Ed. Engl. , vol.33 , pp. 109
  • 22
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    • 2c; see also: Schmalz, H.-G.; Millies, B.; Bats, J.W.; Dürner, G. Angew. Chem. 1992, 104, 640; Angew. Chem., Int. Ed. Engl. 1992, 31, 631.
    • (1992) Angew. Chem., Int. Ed. Engl. , vol.31 , pp. 631
  • 23
    • 85029978152 scopus 로고    scopus 로고
    • note
    • All compounds were fully characterized by the usual spectroscopic methods and gave correct elemental analyses or high resolution MS data; yields refer to analytically pure samples.
  • 26
    • 0001091845 scopus 로고
    • For the use of α-silylated Michael acceptors, see: a) Stork, G.; Ganem, B. J. Am. Chem. Soc. 1973, 95, 6152;
    • (1973) J. Am. Chem. Soc. , vol.95 , pp. 6152
    • Stork, G.1    Ganem, B.2
  • 31
    • 85029987378 scopus 로고    scopus 로고
    • note
    • 7Cr: 59.74 % C, 6.27 % H; found: 59.60 % C 6.29 % H
  • 32
    • 85029978343 scopus 로고    scopus 로고
    • note
    • 1H NMR analysis of the crude product mixture indicated the absence of the typical olefinic proton of the isobutenyl sidechain.
  • 34
    • 85029996135 scopus 로고
    • Schmalz, H.-G.; Siegel, S.; Bats, J.W. Angew. Chem. 1995, 107, 2597; Angew. Chem., Int. Ed. Engl. 1995, 36, 2383.
    • (1995) Angew. Chem., Int. Ed. Engl. , vol.36 , pp. 2383
  • 35
    • 85029974509 scopus 로고    scopus 로고
    • note
    • 10c) and desilylation.
  • 36
    • 85029991889 scopus 로고    scopus 로고
    • note
    • 5Cr: 436.13418, found 436.13418.
  • 40
    • 0001343212 scopus 로고
    • Reviews: a) Kagan, H.B. New J. Chem. 1990, 14, 453; b) Molander, G.A. Chem. Rev. 1992, 92, 26.
    • (1990) New J. Chem. , vol.14 , pp. 453
    • Kagan, H.B.1
  • 41
    • 0040854202 scopus 로고
    • Reviews: a) Kagan, H.B. New J. Chem. 1990, 14, 453; b) Molander, G.A. Chem. Rev. 1992, 92, 26.
    • (1992) Chem. Rev. , vol.92 , pp. 26
    • Molander, G.A.1
  • 42
    • 0000315424 scopus 로고
    • Trost, B.M. (Ed.) Pergamon, Oxford
    • For an excellent general review on radical cyclizations, see: Curran, D.P. in Trost, B.M. (Ed.) Comprehensive Organic Synthesis, Vol. 4, Pergamon, Oxford, 1991, 779.
    • (1991) Comprehensive Organic Synthesis , vol.4 , pp. 779
    • Curran, D.P.1
  • 43
    • 0000900750 scopus 로고
    • Eds. B. M. Trost, I. Fleming, Pergamon, Oxford
    • 3 complexes, see: M.F. Semmelhack in Comprehensive Organic Synthesis, Vol. 4 (Eds. B. M. Trost, I. Fleming), Pergamon, Oxford, 1991, S. 517; and ref. therein.
    • (1991) Comprehensive Organic Synthesis , vol.4 , pp. 517
    • Semmelhack, M.F.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.