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Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100 690. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: int. code + (1223)336-033; e-mail: deposit@ccdc.cam.ac.uk)
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Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100 690. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: int. code + (1223)336-033; e-mail: deposit@ccdc.cam.ac.uk).
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0346765359
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note
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Isonitramine (-)-1 could be obtained in a single step by treating 3 with Raney nickel at 80°C and 25 bar in THF; however, the yield was modest (20%, not optimized).
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19
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