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0001136451
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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84970554539
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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12
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0001577340
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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21344485260
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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Drees, D.1
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14
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21844507605
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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15
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21844508297
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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Mandel, A.1
Magull, J.2
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16
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10044285426
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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Lappert, M.F.1
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17
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0001189310
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and references therein
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Also termed β-diketeniminates and β-aminoiminates, DAP ligands have been known for some time but have recently attracted a surge of interest: a) J. E. Parks, R. H. Holm, Inorg. Chem. 1968, 7, 1408; b) P. C. Healy, M. R. Bendall, D. M. Dodderell, B. W. Skelton, A. H. White, Aust. J. Chem. 1979, 32, 727; c) A. C. Filipou, C. Völkl, R. D. Rogers, J. Organomet. Chem. 1993, 463, 135; d) D. Drees, J. Magull, Z. Anorg. Allg. Chem. 1994, 620, 814; e) ibid. 1995, 621 948; f) A. Mandel, J. Magull, ibid. 1995, 621, 941; g) M. F. Lappert, D.-S. Liu, J. Organomet. Chem. 1995, 500, 203; h) P. B. Hitchcock, J. Hu, M. F. Lappert, M. Layh, D.-S. Liu, J. R. Severn, T. Shu, Anales de Química Int. Ed. 1996, 92, 186, and references therein;
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R. J. Cernik, W. Clegg, C. R. A. Catlow, G. Bushell-Wye, J. V. Flaherty, G. N. Greaves, I. Burrows, D. J. Taylor, S. J. Teat, M. Hamichi, J. Synchrotron Rad. 1997, 4, 279.
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24
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0004150157
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Siemens Analytical X-ray Instruments, Madison WI, USA, version 5 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk)
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-3. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC-100681. Copies of the data can be obtained free of charge on application to CCDC 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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SHELXTL Manual
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Sheldrick, G.M.1
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26
-
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0345395788
-
-
note
-
The only previously reported bridging DAP functions thus through a single, symmetrical N bridge, see ref. [4].
-
-
-
-
27
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33751385924
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D. L. Schulz, B. J. Hinds, D. A. Neumayer., C. L. Stern, T. J. Marks, Chem. Mater., 1993, 1605.
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Marks, T.J.5
-
28
-
-
0344533460
-
-
note
-
Values ranging from 180 to 110° have been previously observed; see ref. [4].
-
-
-
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31
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0000946137
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J. S. Overby, T. P. Hanusa, Angew. Chem. 1994, 106, 2300; Angew. Chem. Int. Ed. Engl. 1994, 33, 2191.
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0001094282
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