메뉴 건너뛰기




Volumn 4, Issue 6, 1998, Pages 1033-1042

Attaching metal-capped sp carbon chains to metal clusters: Synthesis, structure, and reactivity of rhenium/triosmium complexes of formula [(η5-C5Me5)Re(NO)(PPh3)(CC)(n)Os3(CO)(y)(X)(Z)]m+, including carbon geometries more distorted than planar tetracoordinate

Author keywords

Carbon chains; Clusters; Cumulenes; Osmium; Rhenium

Indexed keywords


EID: 0031803654     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3765(19980615)4:6<1033::AID-CHEM1033>3.0.CO;2-P     Document Type: Article
Times cited : (66)

References (67)
  • 1
    • 0000027622 scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1993) Angew. Chem. , vol.105 , pp. 969
    • Beck, W.1    Niemer, B.2    Wieser, M.3
  • 2
    • 33745158307 scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1993) Angew. Chem. Int. Ed. Engl. , vol.32 , pp. 923
  • 3
    • 0000885855 scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1994) Angew. Chem. Int. Ed. Engl. , vol.106 , pp. 569
    • Lang, H.1
  • 4
    • 33748511276 scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1994) Angew. Chem. Int. Ed. Engl. , vol.33 , pp. 547
  • 5
    • 0001283579 scopus 로고    scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1996) Angew. Chem. Int. Ed. Engl. , vol.108 , pp. 1047
    • Bunz, U.1
  • 6
    • 0029789768 scopus 로고    scopus 로고
    • General reviews or perspectives: a) W. Beck, B. Niemer, M. Wieser, Angew. Chem. 1993, 105, 969; Angew. Chem. Int. Ed. Engl. 1993, 32, 923; b) H. Lang, ibid. 1994, 106, 569 and 1994, 33, 547; U. Bunz, ibid. 1996, 108, 1047 and 1996, 35, 969.
    • (1996) Angew. Chem. Int. Ed. Engl. , vol.35 , pp. 969
  • 19
    • 33748243132 scopus 로고
    • b) W. Weng, T. Bartik, J. A. Gladysz, Angew. Chem. 1994, 106, 2272; Angew. Chem. Int. Ed. Engl. 1994, 33, 2199.
    • (1994) Angew. Chem. Int. Ed. Engl. , vol.33 , pp. 2199
  • 26
    • 0038828563 scopus 로고
    • For lead references, see: a) G. H. Worth, B. H. Robinson, J. Simpson, Organometallics 1992, 11, 3863; b) D. Osella, O. Gambino, C. Nevi, M. Ravera, D. Bertolino, Inorg. Chim. Acta 1993, 206, 155.
    • (1992) Organometallics , vol.11 , pp. 3863
    • Worth, G.H.1    Robinson, B.H.2    Simpson, J.3
  • 36
    • 85033875424 scopus 로고
    • Eds.-in-Chief: E. W. Abel, F. G. A. Stone, G. Wilkinson; Volume Eds.: D. F. Shriver, M. I. Bruce, Pergamon, New York, ch. 13.1-13.2
    • A. K. Smith, in Comprehensive Organometallic Chemistry II, Vol. 7 (Eds.-in-Chief: E. W. Abel, F. G. A. Stone, G. Wilkinson; Volume Eds.: D. F. Shriver, M. I. Bruce), Pergamon, New York, 1995, ch. 13.1-13.2.
    • (1995) Comprehensive Organometallic Chemistry II , vol.7
    • Smith, A.K.1
  • 42
    • 2642706854 scopus 로고    scopus 로고
    • note
    • 31P, 23.8, 25.0). In each of these cases, a small third peak (approx. 2%) was also present (ref. [21]).
  • 43
    • 0001537735 scopus 로고
    • 3 signals at δ = 22.0 and 21.6 represent propeller diastereomers: H. Brunner, R. Oeschey, B. Nuber, Angew. Chem. 1994, 106, 941; Angew. Chem., Int. Ed. Engl. 1994, 33, 866.
    • (1994) Angew. Chem. , vol.106 , pp. 941
    • Brunner, H.1    Oeschey, R.2    Nuber, B.3
  • 44
    • 33746311128 scopus 로고
    • 3 signals at δ = 22.0 and 21.6 represent propeller diastereomers: H. Brunner, R. Oeschey, B. Nuber, Angew. Chem. 1994, 106, 941; Angew. Chem., Int. Ed. Engl. 1994, 33, 866.
    • (1994) Angew. Chem., Int. Ed. Engl. , vol.33 , pp. 866
  • 47
    • 6844239208 scopus 로고    scopus 로고
    • -. In order to facilitate comparisons of our data and literature E?⊖ values, we will adopt this convention henceforth.
    • (1996) Chem. Rev. , vol.96 , pp. 877
    • Connelly, N.G.1    Geiger, W.E.2
  • 48
    • 0001117568 scopus 로고    scopus 로고
    • Review: D. Röttger, G. Erker, Angew. Chem. 1997, 109, 840; Angew. Chem. Int. Ed. Engl. 1997, 36, 813.
    • (1997) Angew. Chem. , vol.109 , pp. 840
    • Röttger, D.1    Erker, G.2
  • 49
    • 0001600752 scopus 로고    scopus 로고
    • Review: D. Röttger, G. Erker, Angew. Chem. 1997, 109, 840; Angew. Chem. Int. Ed. Engl. 1997, 36, 813.
    • (1997) Angew. Chem. Int. Ed. Engl. , vol.36 , pp. 813
  • 61
    • 2642679442 scopus 로고    scopus 로고
    • note
    • 3). Stoichiometry based upon integration: a) 0.44 equiv (powder) to 0.46 equiv (crystals); b) 0.25 equiv; c) 0.56 equiv; d) 0.37 equiv; e) 0.57 equiv; f) 0.48 equiv (crystals). All mmol and yield calculations correct for the solvate.
  • 62
    • 2642702781 scopus 로고    scopus 로고
    • Each m/z value is for the most intense peak of the isotope envelope; relative intensities are for the specified mass range
    • Each m/z value is for the most intense peak of the isotope envelope; relative intensities are for the specified mass range.
  • 63
    • 2642638959 scopus 로고    scopus 로고
    • These assignments are provisional
    • These assignments are provisional.
  • 67
    • 2642682603 scopus 로고    scopus 로고
    • 0.5 were deposited in the Cambridge Crystallographic Database upon publication of our preliminary communication (ref. [11])
    • 0.5 were deposited in the Cambridge Crystallographic Database upon publication of our preliminary communication (ref. [11]).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.