Application of extractive heptafluoro-n-butyrylation to hair analysis for methamphetamine and amphetamine

Japanese Journal of Forensic Toxicology

Volumn 16, Issue 3, 1998, Pages 190-199

  Kara, Kenji ^a   Kashimura, Seiichi ^a   Tomojiri, Shigeki ^a   Tanada, Norihiko ^a   Kageura, Mitsuyoshi ^a   Tanaka, Keiichi ^a  

^a FUKUOKA UNIVERSITY   (Japan)

Author keywords

4 Hydroxyamphetamine; 4 Hydroxymethamphetamine; Amphetamine; Extractive derivatization; GC MS; Hair analysis; Heptafluoro n butyrylation; Methamphetamine

Indexed keywords

AMPHETAMINE; HYDROCHLORIC ACID; HYDROXYAMPHETAMINE; METHAMPHETAMINE; PHOLEDRINE;

ARTICLE; DERIVATIZATION; DEVICE; GAS CHROMATOGRAPHY; HAIR ANALYSIS; HUMAN; HUMAN TISSUE; MASS SPECTROMETRY; PH; SUBSTANCE ABUSE;

EID: 0031767565     PISSN: 09159606     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (11)

1. ) Sacks, H. : History of hair analysis. Forensic Sci Int, 84, 7-16 (1997).
2. Nakahara, Y.: Detection and diagnostic interpretation of amphetamines in hair. Forensic Sci Int, 70, 135-153 (1995).
3. Nakahara, Y., Takahashi, K., Takeda, Y., Konuma, K., Fukui, S. and Tokui, T.: Hair analysis for drug abuse, part II. Hair analysis for monitoring of methamphetamine abuse by isotope dilution gas chromatography/mass spectrometry. Forensic Sci Int, 46, 243-254 (1990).
4. Suzuki, O., Hattori, H. and Asano, M.: Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry. J Forensic Sci, 29, 611-617 (1984).
5. Hara, K., Kashimura, S., Hieda, Y. and Kageura, M.: Simple extractive derivatization of methamphetamine and its metabolites in biological materials with Extrelut®columns for their GC-MS determination. J Anal Toxicol, 21, 54-58 (1997).
6. Hara, K., Kageura, M., Hieda, Y. and Kashimura, S.: Simultaneous quantitative analysis of methamphetamine and 4-hydroxymethamphetamine in body fluids by gas chromatography/mass spectrometry. Z Rechtsmed, 100, 231-236 (1988).
7. Ferrito, V., Borg, R., Eagles, J. and Fenwick, G.R.: Gas Chromatographic and mass spectrometric characteristics of 2-trifluoromethyl-3-oxazol-5-ones. A potentially useful derivative for α-amino acids. Biomed Mass Spectrom, 4, 499-501 (1979).
8. Tanada, N., Kageura, M., Kashimura, S. and Hara, K.: A simple and sensitive analysis of oxidation dyes on human hair. In Wakasugi, C. (ed), Advances in Legal Medicine 3, issued by Organizing Committee of the 3rd International Symposium, Advances in Legal Medicine, Osaka Univ. Med. School, Osaka, 1997, pp. 629-631.
9. Valter, S. and Cody, J.T.: Evaluation of internal standards for the analysis of amphetamine and methamphetamine. J Anal Toxicol, 19, 316-322 (1995).
10. Kintz, P. and Cirimele, V.: Interlaboratory comparison of quantitative determination of amphetamine and related compounds in hair samples. Forensic Sci Int, 84, 151-156 (1997).
11. Nagasawa, N., Yashiki, M., Iwasaki, Y., Hara, K. and Kojima,T.: Rapid analysis of amphetamines in blood using head space-solid phase microextraction and selected ion monitoring. Forensic Sci Int, 78, 95-102 (1996).