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2N methylene region between δ = 6.0 and 4.0 was used for determining product distributions. All new compounds were characterized by high-resolution NMR spectroscopy (600 MHz) and high-resolution mass spectrometry.
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21
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15844390881
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note
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-1 was estimated. Solutions of 3 in benzene were analyzed by electrospray mass spectrometry (ESI-MS) and showed, in addition to the signal for monomer 3 at 1268 Da, a fairly strong (ca. 20%) signal for dimer 6 at 2535 Da.
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15844426125
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note
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3, in which the carboxamide is not encapsulated.
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