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n: (a) Brookhart, M.; Wagner, M. I. J. Am. Chem. Soc. 1996, 118, 7219. (b) Brookhart, M.; Wagner, M. L; Balavoine, G. G. A.; Ait Haddou, H. J. Am. Chem. Soc. 1994, 116, 3641. (c) Brookhart, M.; Rix, C. R.; DeSimone, J. M. J. Am. Chem. Soc. 1992, 114, 5894. (d) Corradini, P.; DeRossa, C.; Panuzzi, A.; Petrucci, G; Pino, P. Chimia 1990, 44, 52. (e) Barsacchi, M.; Consiglio, G.; Medici, L., Petrucci, G.; Suter, U. W. Angew. Chem., Int. Ed. Engl. 1991, 30, 989. (f) Drent, E. Eur. Pat. Appl. EP 229,-408, 1986.
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0001447529
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n: (a) Brookhart, M.; Wagner, M. I. J. Am. Chem. Soc. 1996, 118, 7219. (b) Brookhart, M.; Wagner, M. L; Balavoine, G. G. A.; Ait Haddou, H. J. Am. Chem. Soc. 1994, 116, 3641. (c) Brookhart, M.; Rix, C. R.; DeSimone, J. M. J. Am. Chem. Soc. 1992, 114, 5894. (d) Corradini, P.; DeRossa, C.; Panuzzi, A.; Petrucci, G; Pino, P. Chimia 1990, 44, 52. (e) Barsacchi, M.; Consiglio, G.; Medici, L., Petrucci, G.; Suter, U. W. Angew. Chem., Int. Ed. Engl. 1991, 30, 989. (f) Drent, E. Eur. Pat. Appl. EP 229,-408, 1986.
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n: (a) Brookhart, M.; Wagner, M. I. J. Am. Chem. Soc. 1996, 118, 7219. (b) Brookhart, M.; Wagner, M. L; Balavoine, G. G. A.; Ait Haddou, H. J. Am. Chem. Soc. 1994, 116, 3641. (c) Brookhart, M.; Rix, C. R.; DeSimone, J. M. J. Am. Chem. Soc. 1992, 114, 5894. (d) Corradini, P.; DeRossa, C.; Panuzzi, A.; Petrucci, G; Pino, P. Chimia 1990, 44, 52. (e) Barsacchi, M.; Consiglio, G.; Medici, L., Petrucci, G.; Suter, U. W. Angew. Chem., Int. Ed. Engl. 1991, 30, 989. (f) Drent, E. Eur. Pat. Appl. EP 229,-408, 1986.
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33748215494
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n: (a) Brookhart, M.; Wagner, M. I. J. Am. Chem. Soc. 1996, 118, 7219. (b) Brookhart, M.; Wagner, M. L; Balavoine, G. G. A.; Ait Haddou, H. J. Am. Chem. Soc. 1994, 116, 3641. (c) Brookhart, M.; Rix, C. R.; DeSimone, J. M. J. Am. Chem. Soc. 1992, 114, 5894. (d) Corradini, P.; DeRossa, C.; Panuzzi, A.; Petrucci, G; Pino, P. Chimia 1990, 44, 52. (e) Barsacchi, M.; Consiglio, G.; Medici, L., Petrucci, G.; Suter, U. W. Angew. Chem., Int. Ed. Engl. 1991, 30, 989. (f) Drent, E. Eur. Pat. Appl. EP 229,-408, 1986.
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5844391694
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n: (a) Brookhart, M.; Wagner, M. I. J. Am. Chem. Soc. 1996, 118, 7219. (b) Brookhart, M.; Wagner, M. L; Balavoine, G. G. A.; Ait Haddou, H. J. Am. Chem. Soc. 1994, 116, 3641. (c) Brookhart, M.; Rix, C. R.; DeSimone, J. M. J. Am. Chem. Soc. 1992, 114, 5894. (d) Corradini, P.; DeRossa, C.; Panuzzi, A.; Petrucci, G; Pino, P. Chimia 1990, 44, 52. (e) Barsacchi, M.; Consiglio, G.; Medici, L., Petrucci, G.; Suter, U. W. Angew. Chem., Int. Ed. Engl. 1991, 30, 989. (f) Drent, E. Eur. Pat. Appl. EP 229,-408, 1986.
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Drent, E.1
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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Jiang, Z.1
Sen, A.2
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0000232571
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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Sperrle, M.1
Consiglio, G.2
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19
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0028485389
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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Bronco, S.1
Consiglio, G.2
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Batistini, A.4
Suter, U.W.5
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20
-
-
0000909035
-
-
n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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Barsacchi, M.1
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33748227070
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-
n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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5844383379
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U.S. Patent 4,970,294, 1990
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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Drent, E.1
Wife, R.L.2
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23
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0001427029
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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24
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n oligomers and polymers (including polymers with spiroketal units): (a) Jiang, Z.; Sen, A. J. Am. Chem. Soc. 1995, 117, 4455. (b) Sperrle, M.; Consiglio, G. J. Am. Chem. Soc. 1995, 117, 12130. (c) Bronco, S.; Consiglio, G.; Hutter, R. Batistini, A.; Suter, U. W. Macromolecules 1994, 27, 4436. (d) Barsacchi, M.; Batistini, A.; Consiglio, G.; Suter, U. W. Macromolecules 1992, 25, 3604. (e) Batistini, A.; Consiglio, G. Suter, U. W. Angew. Chem., Int. Ed. Engl. 1992, 31, 303. (f) Drent, E.; Wife, R. L. U.S. Patent 4,970,294, 1990. (g) Xu, F. Y.; Zhao, A. X.; Chien, J. C. W. Makromol. Chem. 1993, 194, 2579. (h) Abu-Surrah, A. S.; Wursche, R.; Rieger, B.; Eckert, G.; Pechhold, W. Macromolecules 1996, 29, 4806.
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By contrast, most transition metal catalysts induce ring-opening olefin metathesis polymerization (ROMP) of nor-bornene based monomers leading to polymer structures containing ring-opened repeating units: (a) Novak, B.; Risse, W.; Grubbs, R. H. Advances in Polymer Science; Springer Verlag: New York, 1992; Vol. 102; p 47. (b) Schrock, R. R. Acc. Chem. Res. 1990, 23, 158. (c) Ivin, K. J. Olefin Metathesis, Academic Press: London, 1983.
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The rigid bicyclic structure renders the β-hydrogens inaccessible for β-hydride elimination, thus reducing the rate of chain-transfer reactions.
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Syntheses of 3a - c was performed according to procedures described in: (a) Binger, P. Synthesis 1974, 190. (b) Nesmeyanova, O. A.; Rudashevskaya, T. Y.; Dyachenko, A. I.; Savilova, S. F.; Nesedov, O. M. Synthesis 1982, 296. These three-step monomer syntheses are suitable for laboratory preparations on a scale of up to several grams. The third reaction step is to some degree experimentally demanding and requires high purity starting materials. Different monomer syntheses with potential for scale up are required in order to improve the overall practicality. Other cyclopropene syntheses were described in: (c) Closs, G. L.; Gloss, L. E.; Böll, W. A. J. Am. Chem. Soc. 1963, 85, 3796.
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0001006155
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Syntheses of 3a - c was performed according to procedures described in: (a) Binger, P. Synthesis 1974, 190. (b) Nesmeyanova, O. A.; Rudashevskaya, T. Y.; Dyachenko, A. I.; Savilova, S. F.; Nesedov, O. M. Synthesis 1982, 296. These three-step monomer syntheses are suitable for laboratory preparations on a scale of up to several grams. The third reaction step is to some degree experimentally demanding and requires high purity starting materials. Different monomer syntheses with potential for scale up are required in order to improve the overall practicality. Other cyclopropene syntheses were described in: (c) Closs, G. L.; Gloss, L. E.; Böll, W. A. J. Am. Chem. Soc. 1963, 85, 3796.
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1H NMR spectroscopy in bromobenzene-ds at 80°C.
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66
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5844376303
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note
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Polymer yields decrease when the initial mol ratio of monomer to catalyst is increased (Table 1) due to the unselective nature of the polymerization when catalyst 4 is used.
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67
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5844414680
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note
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Relative number average molecular weights of the parts of poly-3bb′ and poly-3cc′ soluble in chlorobenzene at 20°C (between 60 and 90 wt %); calibration with polystyrene samples.
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1H NMR spectrum of the resulting ring-opened polymer shows the olefinic signal at δ 5.45. The signal due to the cyclopropane ring protons of poly-3a at δ 0.65-0.45 disappears after reaction with 4.
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-
-25c are described in: (a) Byers, P. K.; Canty, A. J.; Traill, P. R.; Watson, A. A. J. Organomet. Chem. 1990, 390, 399. (b) Deeming, A. J.; Rothwell, I. P.; Hursthouse, M. B.; Backer-Dirks, J. D. J. J. Chem. Soc., Chem. Commun. 1979, 670. (c) Crociani, B.; Di Bianca, F.; Uguagliati, P.; Canovese, L.; Berton, A. J. Chem. Soc., Dalton Trans. 1991, 71.
-
(1979)
J. Chem. Soc., Chem. Commun.
, pp. 670
-
-
Deeming, A.J.1
Rothwell, I.P.2
Hursthouse, M.B.3
Backer-Dirks, J.D.J.4
-
83
-
-
4544309445
-
-
-25c are described in: (a) Byers, P. K.; Canty, A. J.; Traill, P. R.; Watson, A. A. J. Organomet. Chem. 1990, 390, 399. (b) Deeming, A. J.; Rothwell, I. P.; Hursthouse, M. B.; Backer-Dirks, J. D. J. J. Chem. Soc., Chem. Commun. 1979, 670. (c) Crociani, B.; Di Bianca, F.; Uguagliati, P.; Canovese, L.; Berton, A. J. Chem. Soc., Dalton Trans. 1991, 71.
-
(1991)
J. Chem. Soc., Dalton Trans.
, pp. 71
-
-
Crociani, B.1
Di Bianca, F.2
Uguagliati, P.3
Canovese, L.4
Berton, A.5
-
84
-
-
0001102772
-
-
Togni, A.; Rihs, G.; Pregosin, P. S.; Ammann, C. Helv. Chim. Acta 1990, 73, 723.
-
(1990)
Helv. Chim. Acta
, vol.73
, pp. 723
-
-
Togni, A.1
Rihs, G.2
Pregosin, P.S.3
Ammann, C.4
-
85
-
-
84987263015
-
-
Similar to: von Matt, P.; Lloyd-Jones, G. C.; Minidis, A. B. E.; Pfaltz, A.; Macko, L.; Neuburger, M.; Zehnder, M.; Rüegger, H.; Pregosin, P. S. Helv. Chim. Acta 1995, 78, 265.
-
(1995)
Helv. Chim. Acta
, vol.78
, pp. 265
-
-
Von Matt, P.1
Lloyd-Jones, G.C.2
Minidis, A.B.E.3
Pfaltz, A.4
Macko, L.5
Neuburger, M.6
Zehnder, M.7
Rüegger, H.8
Pregosin, P.S.9
-
86
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-
5844358351
-
-
note
-
Many of the cyclopropene polymerizations of Table 2 were precipitation polymerizations. As a result, direct relationships between polymer molecular weights and initial mole ratios of monomer to catalyst or polymer yield and reaction time are difficult to establish.
-
-
-
-
87
-
-
5844376304
-
-
note
-
Poly-3a,b samples (entries 7-14) are only partially soluble at 20°C in chlorobenzene.
-
-
-
-
88
-
-
5844414682
-
-
note
-
Chain propagation is being driven by both the release of ring strain and the energy gained from converting a π-bond into a σ-bond.
-
-
-
-
89
-
-
85086527184
-
-
note
-
3 at 20 °C.
-
-
-
-
90
-
-
0029062857
-
-
Barrett, A. G. M.; Kasdorf, K.; Tustin, G. J.: Williams, D. J. J. Chem. Soc., Chem. Commun. 1995, 1143.
-
(1995)
J. Chem. Soc., Chem. Commun.
, pp. 1143
-
-
Barrett, A.G.M.1
Kasdorf, K.2
Tustin, G.J.3
Williams, D.J.4
-
91
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-
0003409730
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-
John Wiley: Chichester, England
-
(a) Kalinowski, H.-O.; Berger, S.; Braun, S. Carbon-13 NMR Spectroscopy, John Wiley: Chichester, England, 1988.
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(1988)
Carbon-13 NMR Spectroscopy
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-
Kalinowski, H.-O.1
Berger, S.2
Braun, S.3
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92
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-
5844381487
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(b) DePuy, C. H.; Fünfschilling, P. C.; Andrist, A. H.; Olson, J. Am. Chem. Soc. 1977, 99, 6297.
-
(1977)
J. Am. Chem. Soc.
, vol.99
, pp. 6297
-
-
DePuy, C.H.1
Fünfschilling, P.C.2
Andrist, A.H.3
Olson4
-
93
-
-
85086525625
-
-
note
-
13C NMR shift difference for Me(cis) and Me(trans) is a result of the rigidity of the polymer structure. There is no rotation about the C-C bonds which are part of the three-membered rings.
-
-
-
-
94
-
-
5844426433
-
-
note
-
5 (of 8). Both Me*(c) (δ 21.7) and Me*(t) (δ 27.8) can be compared with the geminal methyl groups of 1,1,2-trimethylcyclopropane 6f (δ 19.5 and 27.4 in Figure 2) as they experience only two additional δ-effects. Me(t) at δ 29.3 and Me(c) at 17.4 of 8 are in almost the same environment as Me(trans) and Me (cis) of 7. (They differ slightly due to a difference in the shielding/deshielding effects induced by the neighboring terminal cyclopropane units.) (Matrix Presented)
-
-
-
-
95
-
-
85086526504
-
-
note
-
36b However these polycyclopentenes are 1,3-linked polymers in contrast to the present 1,2-linked polycyclopropenes and are not really suited as a model for discussing chain-end control as the exclusive mechanism of stereocontrol.
-
-
-
-
97
-
-
5844350893
-
-
note
-
4a
-
-
-
-
98
-
-
85086527100
-
-
note
-
16a They are the predominant reaction products in addition to small amounts of cyclotrimers and cyclotetramers.
-
-
-
-
99
-
-
85086527822
-
-
note
-
2-carbons of the ethyl substituents show peaks (overlapped by resonances corresponding to the three-membered ring carbons) at δ 23.9-22.9 when they are cis to the polymer main chain (3b,c units) and signals at δ 36.7-36.2 when they are in a trans position (3b,t units).
-
-
-
-
100
-
-
85086527174
-
-
note
-
13C NMR signals are shifted upfield due to the γ-syn effect.
-
-
-
-
101
-
-
85086526150
-
-
note
-
-1 (at 373 K).
-
-
-
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