Thermolysis of benzo[c]phenanthrene-5,6-dicarboxylic anhydride and 6H-benzo[cd]pyren-6-one. Entries to the combustion effluents benzo[ghi]fluoranthene and cyclopenta[cd]pyrene

Tetrahedron Letters

Volumn 38, Issue 26, 1997, Pages 4689-4692

  Sarobe, Martin ^a   Jenneskens, Leonardus W ^a   Wiersum, Ulfert E ^a  

^a UTRECHT UNIVERSITY   (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

BENZO[C]PHENANTHRIDINE DERIVATIVE; FLUORANTHENE; FULLERENE; POLYCYCLIC AROMATIC HYDROCARBON;

ARTICLE; CHEMICAL REACTION; COMBUSTION; DRUG HYDROLYSIS; PRESSURE; TEMPERATURE;

OXY;

EID: 0031005297     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00998-2     Document Type: Article

References (19)

1. Lafleur, A.L.; Howard, J.B.; Taghizadeh, K.; Plummer, E.F.; Scott, L.T.; Necula, A.; Swallow, K.C. J. Phys. Chem., 1996, 100, 17421 and references cited.
2. For a review: Brown, R.F.C. Recl. Trav. Chim. Pays Bas, 1988, 107, 655 and references cited.
3. For a review: Schaden, G. J. Anal. Appl. Pyrol., 1985, 8, 135. and references cited.
4. 8 CP-PAH pyracylene and ethynyl substituted acenaphthylenes: Scott, L.T. Pure & Appl. Chem., 1996, 68, 291.
5. 8 CP-PAH pyracylene and ethynyl substituted acenaphthylenes: Scott, L.T. Pure & Appl. Chem., 1996, 68, 291.
6. Szmuszkovicz, J.; Modest, E.J. J. Am. Chem. Soc., 1948, 70, 2542.
7. Clar, E.; Mackay, C.C. Tetrahedron, 1972, 28, 6041.
8. Studt, P.; Win, T. Liebigs Ann. Chem., 1983, 70, 2542.
9. Sarobe, M.; Zwikker, J.W.; Snoeijer, J.D.; Wiersum, U.E.; Jenneskens, L.W. J. Chem. Soc., Chem. Commun., 1994, 89 and references cited.
10. Ebert, L.B. Science, 1990, 247, 1468; see also Kroto, H.W.; McKay, K. Nature, 1988, 331, 328.
11. Ebert, L.B. Science, 1990, 247, 1468; see also Kroto, H.W.; McKay, K. Nature, 1988, 331, 328.
12. Sarobe, M.; Jenneskens, L.W.; Wiersum, U.E. Tetrahedron Lett., 1996, 37, 1121.
13. Plater, M.J. Tetrahedron Lett., 1994, 35, 6147.
14. Jenneskens, L.W.; Sarobe, M; Zwikker, J.W. Pure & Appl. Chem., 1996, 68, 219.
15. Brown, R.F.C.; Coulston, K.J.; Eastwood, F.W. Tetrahedron Lett., 1996, 37, 6819.
16. 10 no evidence for the formation of the combustion effluent cyclopent[hi]acephenanthrylene even in trace amounts was found.
17. 2 giving rise to larger contact times and more rigorous thermolysis conditions; carbonization in the hot zone becomes a competitive process leading to a decrease in mass recoveries (Table 2). See also: Brown, R.F.C. Pyrolytic Methods in Organic Chemistry, Organic Chemistry Monographs, Academic Press, Vol. 41, New York 1980.
18. Crowley, C.; Taylor, R.; Kroto, H.W.; Walton, D.R.M.; Cheng, P.-C.; Scott, L.T. Synth. Metals, 1996, 77, 17 and references cited; Osterodt, J.; Zett, A.; Vögtle, F. Tetrahedron, 1996, 52, 4949.
19. Crowley, C.; Taylor, R.; Kroto, H.W.; Walton, D.R.M.; Cheng, P.-C.; Scott, L.T. Synth. Metals, 1996, 77, 17 and references cited; Osterodt, J.; Zett, A.; Vögtle, F. Tetrahedron, 1996, 52, 4949.