The synthesis of a novel benzodiazocine via an intramolecular Staudinger/aza-Wittig cyclization

Tetrahedron Letters

Volumn 38, Issue 20, 1997, Pages 3609-3610

  O'Neil, Ian A ^a   Murray, Clare L ^a   Potter, Andrew J ^a   Kalindjian, S Barret ^b  

^a UNIVERSITY OF LIVERPOOL   (United Kingdom)

^b James Black Foundation   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

BENZODIAZOCINE DERIVATIVE; PYRROLE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; DRUG SYNTHESIS; IN VITRO STUDY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION ANALYSIS;

EID: 0030958696     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)00680-1     Document Type: Article

References (9)

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3. O'Neil, I. A.; Murray, C. L.; Hunter, R. C.; Kalindjian, S. B. Synlett, 1997, 75.
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5. Eguchi, S.; Yamashita, K.; Matsushita, Y.; Kakehi, A. J. Org. Chem., 1995, 60, 4006.
6. Kamal, A.; Praveen Reddy, B. S.; Narayan Reddy, B. S. Tet. Lett., 1996, 37, 6803.
7. Balaspiri, L.; Penke, B.; Papp, G.; Dombi, G.; Kovacs, K. Helv. Chim. Acta., 1975, 55, 969.
8. 3. The imine proton is clearly present at δ7.94 and the C11-H (carbinolamine form) at δ4.10ppm. Full NMR details will be reported elsewhere.
9. Jonnson, A. W. Ylides and Imines of Phosphorus, Wiley, New York, 1993.