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For enantiopure α-trifluoromethyl α-amino acids via sulfoxide chemistry: a) Bravo, P.; Capelli, S.; Meille, S. V; Viani, F.; Zanda, M.; Kukhar, V. P.; Soloshonok, V. A. Tetrahedron: Asymmetry 1994, 5, 2009-2018.
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a) Arnone, A.; Bravo, P.; Capelli, S.; Fronza, G.; Meille, S. V.; Zanda, M.; Cavicchio, G.; Crucianelli, M. J. Org. Chem. 1996, 61, 3375-3387.
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note
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Preliminary studies on the Mitsunobu azidation of 1,1,1-trifluoro-, 1-chloro-1,1-difluoro-, and 1,1-difluoro-3-[(4-methylphenyl)sulfinyl]propan-2-ol showed that the corresponding vinylsulfoxides are formed as the main products, the azides being formed in low amount, if any.
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23
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