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note
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2 [17]. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were added in idealized positions and included in the refinement except for the hydroxyl hydrogen atoms in 2, which were located in the difference map and refined with restrained 1-2 distances and a common isotropic U value. The disordered positions of the solvent n-hexane molecule in 2 and the coordinated THF molecule in 3 were refined with the help of distance and ADP-restraints. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publications nos. CCDC-100 133 (2) and CCDC-100 145 (3 and 4). Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: Int. code +(1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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