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2S=S. At sufficiently high temperatures, the possibility of sulfur inversion in the latter derivatives cannot be, in principle, excluded.
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note
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-3 ppm (at -20°C). We also checked that the use of a racemic version of the same alcohol did not provide any splitting.
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21
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37049093686
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-1, or even more than that, depending on the solvent employed; see, for instance: Harris, R. K.; Pryce-Jones, T.; Swinbourne, F. J. J. Chem. Soc., Perkin Trans. 2 1980, 476. Lunazzi, L.; Cerioni, G.; Foresti, E.; Macciantelli, D. J. Chem. Soc., Perkin Trans. 2 1978, 686. Anet, F. A. L.; Ji, X. Tetrahedron Lett. 1984, 25, 1419. Lunazzi, L.; Magagnoli, C.; Guerra, M.; Macciantelli, D. Tetrahedron Lett. 1979, 3031.
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-1, or even more than that, depending on the solvent employed; see, for instance: Harris, R. K.; Pryce-Jones, T.; Swinbourne, F. J. J. Chem. Soc., Perkin Trans. 2 1980, 476. Lunazzi, L.; Cerioni, G.; Foresti, E.; Macciantelli, D. J. Chem. Soc., Perkin Trans. 2 1978, 686. Anet, F. A. L.; Ji, X. Tetrahedron Lett. 1984, 25, 1419. Lunazzi, L.; Magagnoli, C.; Guerra, M.; Macciantelli, D. Tetrahedron Lett. 1979, 3031.
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