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Volumn 38, Issue 42, 1997, Pages 7329-7332

Studies on the total synthesis of the macrolide antitumor agent rhizoxin. 1. Synthesis of the C3-C13 segment

Author keywords

[No Author keywords available]

Indexed keywords

ANTINEOPLASTIC AGENT; RHIZOXIN;

EID: 0030768734     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)01780-2     Document Type: Article
Times cited : (26)

References (31)
  • 6
    • 0029033724 scopus 로고
    • b) Nakada, M.; Kobayashi, S.; Shibasaki, M.; Iwasaki, S.; Ohno, M. Tetrahedron Lett. 1993, 34, 1039. For the total synthesis of didesepoxyrhizoxin, see: Kende, A.S.; Blass, B.E.; Henry, J.R. Tetrahedron Lett. 1995, 36, 4741.
    • (1995) Tetrahedron Lett. , vol.36 , pp. 4741
    • Kende, A.S.1    Blass, B.E.2    Henry, J.R.3
  • 17
    • 0027209655 scopus 로고
    • Keck, G.E.; Park, M.; Krishnamurthy, D. J. Org. Chem. 1993, 58, 3787. See also, Linderman, R.J.; Cusack, K.P.; Jaber, M.R. Tetrahedron Lett. 1996, 37, 6649.
    • (1993) J. Org. Chem. , vol.58 , pp. 3787
    • Keck, G.E.1    Park, M.2    Krishnamurthy, D.3
  • 22
    • 0343520838 scopus 로고    scopus 로고
    • This procedure facilitated removal (by flash chromatography) of a small quantity of the primary p-nitrobenzoate that resulted from ester migration during cleavage of the benzyl ether
    • This procedure facilitated removal (by flash chromatography) of a small quantity of the primary p-nitrobenzoate that resulted from ester migration during cleavage of the benzyl ether.
  • 24
    • 0343084782 scopus 로고    scopus 로고
    • note
    • 6ax J=11 Hz) and the proton at C7 of 5%.
  • 30
    • 0343520833 scopus 로고    scopus 로고
    • note
    • 3) δ 0.22 (9 H, s), 0.96-1.0 (3 H, m), 1.08-1.23 (2 H, m), 1.80-1.95 (5 H, m), 2.09 (1 H, d, J=10.5 Hz), 2.26-2.61 (3 H, m), 4.02-4.16 (1 H, m), 4.79 (1 H, s), 5.61-5.71 (1 H, m), 5.73 (1 H, d, J=5.6 Hz), 6.10-6.30 (2 H, m), 7.22-7.35 (3 H, m), 7.45 (2 H, d, J=7.6 Hz).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.