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The following abbreviations were used for solvents, reagents, compound names, etc... DCM = dichloromethane; DMF = dimethylformamide; DMSO = dimethylsulfoxide; THF = tetrahydrofuran; TFA = trifluoroacetic acid; TIPS = triisopropylsilane DIEA = diisopropylethylamine; DMAP = 4-dimethylaminopyridine; DCC = N,N'-dicyclohexylcarbodiimide; DCU = dicyclohexylurea; DIC = N,N'-diisopropylcarbodiimide; HOBt = N-hydroxybenzotriazole; PyBOP = benzotriazole-l-yl-oxy-tris-pyrrolidino-phosphonium hexafluorophosphate; Fmoc = 9-fluorenylmethoxycarbonyl RP-HPLC = reverse phase high performance liquid chromatography; NMR = nuclear magnetic resonance; FT-ICR = Courier transform - ion cyclotron resonance; t.l.c. = thin layer chromatography (chloroform:ethyl acetate (9:1); Ac = acetyl; A = Ala = alanine; K = Lys = lysine; G = Gly = glycine; Glu = glutamic acid; eq = equivalents; nm = nanometers
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