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1842409431
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note
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3) have been recorded. A detailed examination of these diffraction patterns shows that Rbpen V is essentially isomorphous and isostructural with KpenV both above and below the phase change at ∼365 K
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M. D. Phil Thesis, University of Oxford, Wendeler, M.; Heyes, S. J. Unpublished results
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37
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1842415282
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note
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1H dipolar broadening regime; the absence of any positional disorder in the X-ray crystal structures - all these observations are consistent with 180° ring flip motions as the single most significant dynamic process in these crystals.
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38
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1842403402
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note
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27
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39
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0000570050
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40
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1842407051
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note
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13C CP/MAS NMR spectrum, which is identical to that of the sample prior to heating.
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