Pulsed field gradient 'inverse' HOESY applied to the isotope pairs 1H,31P and 1H,7Li

Magnetic Resonance in Chemistry

Volumn 34, Issue 7, 1996, Pages 532-537

  Bauer, Walter ^a  

^a UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

Author keywords

1H NMR; 31P NMR; 7Li NMR; Inverse HOESY; N butyllithium; NMR; Pulsed field gradients; Thytnolphthalein

Indexed keywords

INVERSE PROBLEMS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

1H NMR; 31P-NMR; 7LI NMR; HETERONUCLEAR OVERHAUSER EFFECTS; INVERSE HETERONUCLEAR OVERHAUSE EFFECT SPECTROSCOPY; ISOTOPE PAIR; N-BUTYLLITHIUM; NOISE ARTIFACTS; PULSED FIELD GRADIENTS; THYTNOLPHTHALEIN;

NUCLEAR MAGNETIC RESONANCE;

EID: 0030560102     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199607)34:7<532::AID-OMR910>3.0.CO;2-C     Document Type: Article

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8. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
9. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
10. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
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12. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
13. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
14. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
15. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
16. W. Bauer, in Lithium Chemistry: a Theoretical and Experimental Overview, edited by A.-M. Sapse and P. v. R. Schleyer. Wiley, New York (1995); W. Bauer, in Advances in Carbanion Chemistry, edited by V. Snieckus. Jai Press, Greenwich, CT (1992); L. A. Paquette, M. R. Sivik, W. Bauer and P. v. R. Schleyer, Organometallics 13, 4919 (1994); W. Bauer and L. Lochmann, J. Am. Chem. Soc. 114, 7482 (1992); W. Bauer and F. Hampel, J. Chem. Soc., Chem. Commun. 903 (1992); W. Bauer, G. A. O'Doherty, P. v. R. Schleyer and L. A. Paquette, J. Am. Chem. Soc. 113, 7093 (1991); L. A. Paquette, W. Bauer, M. R. Sivik, M. Bühl, M. Feigel and P. v. R. Schleyer, J. Am. Chem. Soc. 112, 8776 (1990); D. Hoffmann, W. Bauer and P. v. R. Schleyer, J. Chem. Soc., Chem. Commun. 208 (1990) ; W. Bauer and P. v. R. Schleyer, J. Am. Chem. Soc. 111, 7191 (1989); W. Bauer and P. v. R. Schleyer, Magn. Reson. Chem. 26, 827 (1988); W. Bauer, M. Feigel, G. Müller and P. v. R. Schleyer, J. Am. Chem. Soc. 110, 6033 (1988); H. Balzer and S. Berger, Chem. Ber. 125, 733 (1992); H. Ahlbrecht, J. Harbach, T. Hauck and H.-O. Kalinowski, Chem. Ber. 125, 1753 (1992); G. T. DeLong, D. K. Pannell, M. T. Clarke and R. D. Thomas, J. Am. Chem. Soc. 115, 7013 (1993); T. Ruhland, R. W. Hoffmann, S. Schade and G. Boche, Chem. Ber. 128, 551 (1995); G. Hilmersson and Ö. Davidsson, Organometallics 14, 912 (1995); G. Hilmersson and Ö. Davidsson, J. Org. Chem. 60, 7660 (1995).
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