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2 by the same reaction using pentane instead of THF as the solvent and for its use in the synthesis of π-allyl complexes, see: Betz, P.; Döhring, A.; Emrich, R.; Goddard, R.; Jolly, P. W.; Krüger, C.; Romao, C. C.; Schönfelder, K. U.; Tsay, Y. H. Polyhedron 1993, 12, 2651-2662 and literature cited.
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Complete silylation could not be reached. This seems to be a limiting factor for the number of turnovers.
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Complete silylation could not be reached. This seems to be a limiting factor for the number of turnovers.
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