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85030186602
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note
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Gas evolution was noted when 13 melted (reference 7). (formula presented)
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14
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33751553196
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15
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22944457014
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formula presented
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Reduction of the nitroaldehyde with zinc in aqueous acetic acid gave some imine (ca. 25% yield) consistent with the synthesis of 1Δ-pyrroline 1-oxides from 4-nitroaldehydes (Equation 5). See Bonnett, R.; Brown, R. F. C.; Clark, V.M.; Sutherland, I. O.; Todd, A. J. Chem. Soc. 1959, 2094-2102. (formula presented)
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Bonnett, R.1
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Sutherland, I.O.4
Todd, A.5
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17
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0025747958
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Tetrahydrobenzazepines have been synthesized by other routes. See, for example, Grunewald, G. L.; Paradkar, V. M.; Stillions, D. M.; Ching, F. J. Heterocycl. Chem. 1991, 28, 1587-1592.
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Ching, F.4
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18
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0030063098
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Thomas, C. E.; Ohlweiler, D. F.; Carr, A. A.; Nieduzak, T. R.,; Hay, D. A.; Adams, G.; Vaz, R.; Bemotas, R. C. J. Biol. Chem. 1996, 277, 3097-3104.
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Thomas, C.E.1
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Adams, G.6
Vaz, R.7
Bemotas, R.C.8
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