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34
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0042094151
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note
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16OSi: C, 66.61; H, 8.94. Found: C, 66.89; H, 8.93.
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35
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0010640653
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(a) Dale, J. A.; Dull, D. L.; Mosher, H. S. J. Org. Chem. 1969, 34, 2543-2549.
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37
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0043095978
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note
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Optically pure 9 is a low melting, crystalline solid, whereas the racemate is an oil. Alcohol 9 apparently crystallizes as a conglomerate, which will facilitate the preparation of optically pure samples.
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39
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0041593146
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note
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See Supporting Information for details.
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40
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0043095974
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note
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3 deprotection was less reliable than the TBAF deprotection, and the yields varied from substrate to substrate.
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