Synthesis of dimethyl gloiosiphone A

Synlett

Volumn , Issue 12, 1998, Pages 1357-1358

  Hashizume, Yoshinobu ^a   Maki, Shojiro ^a   Ohashi, Mamoru ^a   Niwa, Haruki ^a  

^a UNIVERSITY OF ELECTRO COMMUNICATIONS   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0008174161     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1998-1987     Document Type: Article

References (15)

1. Chen, J. L.; Moghaddam, M. F.; Gerwick, W. H. J. Nat. Prod. 1993, 56, 1205.
2. (a) Paquette, L. A.; Sturino, C. F.; Doussot, P. J. Am. Chem. Soc. 1996, 118, 9456.
3. (b) Sturino, C. F.; Doussot, P.; Paquette, L. A. Tetrahedron 1997, 53, 8913.
4. Hashizume, Y.; Maki, S.; Ohashi, M.; Niwa, H. Synth. Commun. in press.
5. +]: 209.1178.
6. McCormick, J. P.; Tomasik, W.; Johnson, M. W. Tetrahedron Lett. 1981, 22, 607.
7. α-Hydroxylation of 4a utilizing Davis' procedure resulted in low yield: Davis, F. A.; Vishwakarma, L. C.; Billmers, J. M.; Finn, J. J. Org. Chem. 1984, 49, 3241.
8. +]: 225.1127. The stereochemistry of S was determined by NOE measurement using the derived TES ether A. (Chemical Equation Presented)
9. +): 252.1362.
10. +): 208.1100.
11. (a) Grieco, P. A.; Nishizawa, M.; Oguri, T.; Burke, S. D.; Marinovic, N. J. Am. Chem. Soc. 1977, 99, 5773.
12. (b) Newman, H. J. Org. Chem. 1970, 35, 3990.
13. 2O)+]: 238.1205.
14. +]: 255.1233.
15. +): 23.1205.